Determination of trace germanium in marine sediments by hydride generation-atomic fluorescence spectrometry (HG-AFS)

被引：2
|
作者：
Jing Li
Shilan Zhao
Zhaohui Zhang
Xianjie Zeng
机构：
[1] Ocean University of China,
[2] Environment Protection Administration of Jiaonan City,undefined
来源：
Journal of Ocean University of China | 2004年 / 3卷 / 2期
关键词：
hydride generation-atomic fluorescence spectrometry (HG-AFS); germanium; marine sediment; trace;
D O I：
10.1007/s11802-004-0032-9
中图分类号：
学科分类号：
摘要：
A method for the analysis of trace germanium in marine sediments by HG-AFS has been investigated. The experimental conditions such as the acidity of reduction reaction, the amount of sodium boro-hydride, the carrier gas flow rate, etc., were tested and optimized by using a kind of orthogonal design. The detection limit of the presented method is 0.95µgL1 for germanium. The calibration curve shows a satisfactory line in the concentration range 0–320µgL−1 Ge with a variation coefficient of ±2.1%.
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页码：179 / 182
页数：3
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