Synthesis of sulfolanooctahydrochromenones from 2-benzylidene-3-methyl-4-nitro-2,5-dihydrothiophene 1,1-dioxides

被引:0
|
作者
Igor I. Savelev
Irina E. Efremova
Lidiya V. Lapshina
Vladislav V. Gurzhiy
Ruslan I. Baichurin
机构
[1] Herzen State Pedagogical University of Russia,
[2] S. M. Kirov Military Medical Academy,undefined
[3] Saint Petersburg State University,undefined
来源
Chemistry of Heterocyclic Compounds | 2022年 / 58卷
关键词
2-benzylidene-3-methyl-4-nitro-2,5-dihydrothiophene 1,1-dioxides; enolizable cyclic СН acids; sulfolenes; tandem process;
D O I
暂无
中图分类号
学科分类号
摘要
The reactions of 2-benzylidene-3-methyl-4-nitro-2,5-dihydrothiophene 1,1-dioxides with dimedone were used to synthesize a series of tricyclic compounds containing fused nitrosulfolane and octahydrochromenone rings. The structural features of the obtained polycyclic compounds were established on the basis of IR and NMR spectra, as well as X-ray structural analysis.
引用
收藏
页码:58 / 63
页数:5
相关论文
共 50 条
  • [1] Synthesis of sulfolanooctahydrochromenones from 2-benzylidene-3-methyl-4-nitro-2,5-dihydrothiophene 1,1-dioxides
    Savelev, Igor I.
    Efremova, Irina E.
    Lapshina, Lidiya V.
    Gurzhiy, Vladislav V.
    Baichurin, Ruslan I.
    CHEMISTRY OF HETEROCYCLIC COMPOUNDS, 2022, 58 (01) : 58 - 63
  • [2] Synthesis of sulfolanopyranochromenones by the reaction of 2-benzylidene-3-methyl-4-nitro-2,5-dihydrothiophene 1,1-dioxides with 4-hydroxycoumarin
    Irina E. Efremova
    Igor I. Savelev
    Ruslan I. Baichurin
    Vladislav V. Gurzhiy
    Chemistry of Heterocyclic Compounds, 2022, 58 : 449 - 453
  • [3] Synthesis of sulfolanopyranochromenones by the reaction of 2-benzylidene-3-methyl-4-nitro-2,5-dihydrothiophene 1,1-dioxides with 4-hydroxycoumarin
    Efremova, Irina E.
    Savelev, Igor I.
    Baichurin, Ruslan, I
    Gurzhiy, Vladislav V.
    CHEMISTRY OF HETEROCYCLIC COMPOUNDS, 2022, 58 (8-9) : 449 - 453
  • [4] Modified synthesis and structural features of 2-benzylidene-4-nitro-2,5-dihydrothiophene 1,1-dioxides
    Igor I. Savelev
    Irina E. Efremova
    Lidiya V. Lapshina
    Vladislav V. Gurzhiy
    Alexander V. Belyakov
    Chemistry of Heterocyclic Compounds, 2021, 57 : 861 - 865
  • [5] Modified synthesis and structural features of 2-benzylidene-4-nitro-2,5-dihydrothiophene 1,1-dioxides
    Savelev, Igor I.
    Efremova, Irina E.
    Lapshina, Lidiya V.
    Gurzhiy, Vladislav V.
    Belyakov, Alexander V.
    CHEMISTRY OF HETEROCYCLIC COMPOUNDS, 2021, 57 (7-8) : 861 - 865
  • [6] Reactions of 2-benzylidene-3-methyl-4-nitro-2,5-dihydrothiophene 1,1-dioxide with CH acids
    V. M. Berestovitskaya
    M. V. Selivanova
    M. I. Vakulenko
    I. E. Efremova
    G. A. Berkova
    Russian Journal of Organic Chemistry, 2009, 45 : 1814 - 1817
  • [7] Reactions of 2-benzylidene-3-methyl-4-nitro-2,5-dihydrothiophene 1,1-dioxide with CH acids
    Berestovitskaya, V. M.
    Selivanova, M. V.
    Vakulenko, M. I.
    Efremova, I. E.
    Berkova, G. A.
    RUSSIAN JOURNAL OF ORGANIC CHEMISTRY, 2009, 45 (12) : 1814 - 1817
  • [8] Ir/BiphPHOX-catalyzed asymmetric hydrogenation of 3-substituted 2,5-dihydropyrroles and 2,5-dihydrothiophene 1,1-dioxides
    Meng, Ke
    Xia, Jingzhao
    Wang, Yanzhao
    Zhang, Xinghua
    Yang, Guoqiang
    Zhang, Wanbin
    ORGANIC CHEMISTRY FRONTIERS, 2017, 4 (08): : 1601 - 1605
  • [9] PHOSPHORYLATED 2,5-DIHYDROTHIOPHENE 1,1-DIOXIDES BY 1,4-CYCLOADDITION OF SULFUR-DIOXIDE TO ALKATRIENYLPHOSPHONIC DIALKYL ESTERS
    ENCHEV, DD
    ANGELOV, CM
    KIRILOV, M
    CHEMICA SCRIPTA, 1987, 27 (02): : 295 - 296
  • [10] CONVERSION OF 2,5-DIHYDROTHIOPHENE 1,1-DIOXIDES INTO HIGHLY FUNCTIONALIZED (ETA-4-BUTA-1,3-DIENE)TRICARBONYLIRON(0) COMPLEXES
    YEH, MCP
    CHOU, TS
    TSO, HH
    TSAI, CY
    JOURNAL OF THE CHEMICAL SOCIETY-CHEMICAL COMMUNICATIONS, 1990, (13) : 897 - 898