Crossed-discs of mesoporous silica SBA-15 and their carbon replicas

被引:0
|
作者
Feng Li
Jin-Gui Wang
Yu-Ping Liu
Hui-Jing Zhou
Tie-Hong Chen
机构
[1] Nankai University,Institute of New Catalytic Materials Science, Key Laboratory of Energy
来源
关键词
TMOS; Silica Source; Condensation Rate; Carbon Replica; Silica Wall;
D O I
暂无
中图分类号
学科分类号
摘要
Crossed-discs of mesoporous silica SBA-15 were synthesized by using tetramethylorthosilicate (TMOS) as silica source in the presence of Sn2+ cations. The silica crossed-discs were characterized by small-angle X-ray scattering (SAXS), scanning electron microscopy (SEM), transmission electron microscopy (TEM), and nitrogen adsorption. All the results show that the materials have hexagonally ordered channels running parallel to the thickness of the discs. The effects of the reaction conditions on the morphology of the materials were discussed. The SBA-15 crossed-discs were used as hard templatesto obtain their carbon replicas.
引用
下载
收藏
页码:6505 / 6511
页数:6
相关论文
共 50 条
  • [1] Crossed-discs of mesoporous silica SBA-15 and their carbon replicas
    Li, Feng
    Wang, Jin-Gui
    Liu, Yu-Ping
    Zhou, Hui-Jing
    Chen, Tie-Hong
    JOURNAL OF MATERIALS SCIENCE, 2009, 44 (24) : 6505 - 6511
  • [2] Synthesis of ordered micro-mesoporous carbons by activation of SBA-15 carbon replicas
    Enterria, M.
    Suarez-Garcia, F.
    Martinez-Alonso, A.
    Tascon, J. M. D.
    MICROPOROUS AND MESOPOROUS MATERIALS, 2012, 151 : 390 - 396
  • [3] On the mechanical stability of mesoporous silica SBA-15
    Chytil, Svatopluk
    Haugland, Lise
    Blekkan, Edd A.
    MICROPOROUS AND MESOPOROUS MATERIALS, 2008, 111 (1-3) : 134 - 142
  • [4] A study of morphology of mesoporous silica SBA-15
    Chao, MC
    Lin, HP
    Sheu, HS
    Mou, CY
    NANOPOROUS MATERIALS III, 2002, 141 : 387 - 394
  • [5] Nitridation mechanism of mesoporous silica: SBA-15
    Chino, N
    Okubo, T
    MICROPOROUS AND MESOPOROUS MATERIALS, 2005, 87 (01) : 15 - 22
  • [6] Encapsulation of cellulase with mesoporous silica (SBA-15)
    Takimoto, Anri
    Shiomi, Toru
    Ino, Keita
    Tsunoda, Tatsuo
    Kawai, Akiko
    Mizukami, Fujio
    Sakaguchi, Kengo
    MICROPOROUS AND MESOPOROUS MATERIALS, 2008, 116 (1-3) : 601 - 606
  • [7] Structure sensitivity of vibrational spectra of mesoporous silica SBA-15 and Pt/SBA-15
    Borodko, Y
    Ager, JW
    Marti, GE
    Song, H
    Niesz, K
    Somorjai, GA
    JOURNAL OF PHYSICAL CHEMISTRY B, 2005, 109 (37): : 17386 - 17390
  • [8] SBA-15 templated-ordered mesoporous carbon: effect of SBA-15 microporosity
    Yang, Y
    Sayari, A
    NANOPOROUS MATERIALS IV, 2005, 156 : 543 - 550
  • [9] SBA-15 templated mesoporous carbon: New insights into the SBA-15 pore structure
    Sayari, A
    Yang, Y
    CHEMISTRY OF MATERIALS, 2005, 17 (24) : 6108 - 6113
  • [10] Deposition of Pd into mesoporous silica SBA-15 using supercritical carbon dioxide
    Morere, J.
    Tenorio, M. J.
    Torralvo, M. J.
    Pando, C.
    Renuncio, J. A. R.
    Cabanas, A.
    JOURNAL OF SUPERCRITICAL FLUIDS, 2011, 56 (02): : 213 - 222