Phosphorylation of Betti Base with Bis(diethylamino)phosphoryl Chloride

被引：0
|
作者：
K. E. Metlushka
D. N. Sadkova
K. A. Nikitina
Z. R. Yamaleeva
K. A. Ivshin
O. N. Kataeva
V. A. Alfonsov
机构：
[1] Russian Academy of Sciences,A.E. Arbuzov Institute of Organic and Physical Chemistry, FRC Kazan Scientific Center
[2] Kazan (Volga Region) Federal University,Butlerov Chemical Institute
来源：
Russian Journal of General Chemistry | 2018年 / 88卷
关键词：
Betti base; phosphorylation; thiourea;
D O I：
暂无
中图分类号：
学科分类号：
摘要：
The reaction of bis(diethylamino)phosphoryl chloride with N-Boc-protected 1-(α-aminobenzyl)-2- naphthol (Betti base) proceeded via O-phosphorylation of the phenolic OH group to form the target product as trifluoroacetate salt. The latter reacted with O,O-diethyl thiophosphorylisothiocyanate to give thiourea bearing a chiral Betti base fragment.
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页码：2453 / 2456
页数：3
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