Determination of oxygenated polycyclic aromatic compounds in airborne particulate organic matter using gas chromatography-tandem mass spectrometry

被引:0
|
作者
S. Nicol
J. Dugay
M. -C. Hennion
机构
[1] Ecole Supérieure de Physique et de Chimie Industrielles de Paris,Laboratorie Environnement et Chimie Analytique
来源
Chromatographia | 2001年 / 53卷
关键词
Gas chromatography; Particulate matter; Oxygenated polycyclic aromatic compounds; Tandem mass spectrometry; Collision induced dissociation;
D O I
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中图分类号
学科分类号
摘要
O-PAHs have been analyzed in extracts of particulate matter by GC-MS-MS and GC-MS. Using GC-MS, most O-PAHs could not be detected in raw extracts, or their confirmation was uncertain due to interfering compounds from the matrix. Detection and quantification was greatly improved by using GC-MS-MS. Linearity was observed in the range from 10 to 1000 pg injected. Low traces of O-PAHs, in the range of a few pg·m−3 of air, could be detected without purification or fractionation of the extract.
引用
收藏
页码:S464 / S469
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