Synthesis and Characterization of New Zinc(II) Coordination Polymer with a Flexible Hetro-coordination Ligand via In Situ Reaction as a New Precursor for Zinc(II) Oxide Nano-sphere Particles

被引：0
|
作者：
Mohammad Sadegh Yazdan Parast
Ali Morsali
机构：
[1] Tarbiat Modares University,Department of Chemistry, Faculty of Sciences
来源：
Journal of Inorganic and Organometallic Polymers and Materials | 2012年 / 22卷
关键词：
Zinc(II) coordination polymer; Nanostructure; Zinc(II) oxide;
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摘要：
A new coordination polymer, [Zn3(tza)3(H2O)3]n (1) which H2tza = 1H-tetrazolate-5-acetic acid has been synthesized and characterized by IR spectroscopy, elemental analysis X-ray crystallography. The single-crystal X-ray data of compound 1 show existence of three different ZnII ion with different coordination spheres, hexagonal, pyramidal and pentagonal. This coordination polymer used as a precursor for preparation of zinc(II) oxide nano-particles. Nano-particles were characterized by powder X-ray powder diffraction and the its morphology characterized by scanning electron microscope.
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页码：998 / 1002
页数：4
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