Novel Experimental Approach to Obtain the Oxygen-Deficient LaBaCaCu3Oy Superconductor Compound

被引:0
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作者
M. H. Arada
A. Amira
机构
[1] MSB University,Laboratoire d’étude des matériaux
[2] MSB University,Laboratoire des Essais Non Destructif
关键词
Nitrate decomposition method; X-ray diffraction (XRD); Energy-dispersive analysis with X-rays (EDAX); Superconductors;
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摘要
This work presents a novel approach based on the nitrate decomposition method for the preparation the oxygen-deficient LaBaCaCu3Oy (La1113) compound. The XRD results reveal the presence of the triple perovskite structure LaBaCaCu3Oy as a dominant phase crystallizing in the tetragonal system with the space group P4/mmm. The SEM observation shows a low porosity and EDAX data indicates the presence of the basic elements of the phase. The superconducting character of the compound is confirmed by AC susceptibility measurements with Tc = 63 K even if the samples are not treated under oxygen atmosphere.
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页码:3029 / 3032
页数:3
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