Formation of nanocrystalline Fe73.5Cu1Nb3Si13.5B9 alloy under high pressure

被引:0
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作者
Xiangyi Zhang
Jingwu Zhang
Fuxiang Zhang
Wen Yu
Duanwei He
Liming Cao
Jianhua Zhao
Riping Liu
Yingfan Xu
Wenkui Wang
机构
[1] Chinese Academy of Sciences,Institute of Physics
[2] Yanshan University,College of Materials Science and Engineering
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关键词
high pressure; nanocrystalline alloy; Fe; Cu; Nb; Si; B; alloy;
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学科分类号
摘要
The formation of nanocrystalline Fe73.5 Cu1Nb3Si13.5 B9 alloy by annealing an amorphous Fe73.5Cu1Nb3Si13.5B9 alloy at a temperature of 823 K under pressures in the range of 1–5 GPa is investigated by using X-ray diffraction, electron diffraction, and transmission electron microscopy. The high pressure experiments are carried out in belt-type pressure apparatus. Experimental results show that the initial crystalline phase in these annealed alloys is a-Fe solid solution (named a-Fe phase below), and high pressure has a great influence on the crystallization process of the a-Fe phase. The grain size of the a-Fe phase decreases with the increase of pressure (P). The volume fraction of the a-Fe phase increases with increasing the pressure as the pressure is below 2 GPa, and then decreases (Pδ2 GPa). The mechanism for the effects of the high pressure on the crystallization process of amorphous Fe73.5Cu1Nb3Si13.5B9 alloy is discussed
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页码:407 / 413
页数:6
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