On-line Analysis of Catalytic Reaction Products Using a High-Pressure Tandem Micro-reactor GC/MS

被引：0

作者：

Atsushi Watanabe

Young-Min Kim

Akihiko Hosaka

Chuichi Watanabe

Norio Teramae

Hajime Ohtani

Seungdo Kim

Young-Kwon Park

Kaige Wang

Robert R. Freeman

机构：

[1] Frontier Laboratories Ltd.,Department of Environmental Sciences and Biotechnology

[2] Hallym University,Department of Chemistry, Graduate School of Science

[3] Tohoku University,Department of Materials Science and Engineering, Graduate School of Engineering

[4] Aoba,School of Environmental Engineering

[5] Nagoya Institute of Technology,RTI International

[6] University of Seoul,undefined

[7] 3040 Cornwallis,undefined

[8] Research Triangle Park,undefined

[9] Frontier Laboratories USA,undefined

来源：

Analytical Sciences | 2017年 / 33卷

关键词：

On-line GC/MS analysis; catalytic fast pyrolysis; hydrodeoxygenation; guaiacol; tandem micro-reactor; restrictor capillary tube;

D O I：

暂无

中图分类号：

学科分类号：

摘要：

When a GC/MS system is coupled with a pressurized reactor, the separation efficiency and the retention time are directly affected by the reactor pressure. To keep the GC column flow rate constant irrespective of the reaction pressure, a restrictor capillary tube and an open split interface are attached between the GC injection port and the head of a GC separation column. The capability of the attached modules is demonstrated for the on-line GC/MS analysis of catalytic reaction products of a bio-oil model sample (guaiacol), produced under a pressure of 1 to 3 MPa.

引用

页码：1085 / 1089

页数：4

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