Magnetic Properties and Crystallization of the Fe75Si15B10 Amorphous Alloy Prepared by Mechanical Alloying

被引：0
|
作者：
J. Quispe Marcatoma
V. A. Peña Rodríguez
E. M. Baggio-Saitovitch
机构：
[1] Universidad Nacional Mayor de San Marcos,Facultad de Ciencias Físicas
[2] Centro Brasileiro de Pesquisas Físicas,undefined
来源：
Hyperfine Interactions | 2003年 / 148-149卷
关键词：
mechanical alloying; metallic alloys; soft magnetic materials; Mössbauer spectroscopy;
D O I：
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中图分类号：
学科分类号：
摘要：
The magnetic order and crystallization of the amorphous Fe75Si15B10 alloy prepared by mechanical alloying was studied in situ by 57Fe Mössbauer spectroscopy. These measurements were carried out using a vacuum furnace, controlling the temperature in the absorber. From Mössbauer measurements the magnetic order temperature of the as-milled sample was estimated at about 675 K. In order to identify the crystalline phases formed during heating, Mössbauer measurements were analyzed together with X-ray diffraction analysis. Both results show the formation of several crystalline phases such as Fe5SiB2, Fe2B, Fe3Si, α-Fe, Fe–B composite and a residual amorphous phase.
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页码：97 / 102
页数：5
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