Microcolumn HPLC-UV Analysis of Glycyrrhiza Uralensis and Licorice Preparations

被引：0
|
作者：
D. N. Olennikov
I. N. Zilfikarov
Cecile Vennos
机构：
[1] Institute of General and Experimental Biology Siberian Branch,
[2] Russian Academy of Sciences,undefined
[3] Scientific Center of Biomedical Technologies,undefined
[4] All-Russia Research Institute of Medicinal and Aromatic Plants (VILAR),undefined
[5] Regulatory and Medical Scientific Affairs,undefined
来源：
Pharmaceutical Chemistry Journal | 2019年 / 52卷
关键词：
microcolumn HPLC-UV; flavonoids; chalcones; triterpenes; standardization;
D O I：
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中图分类号：
学科分类号：
摘要：
A microcolumn HPLC method with UV detection (MC-HPLC-UV) using ProntoSIL-120-5-C18 sorbent (1 × 60 mm, 1 μm) and gradient elution by LiClO4(4.1 M)/HClO4(0.1 M)–MeCN was developed for quantitative analysis of seven compounds (liquiritin-2″-O-glucoside, liquiritin, isoliquiritin-2″-O-apioside, isoliquiritin, licorice-saponin G2, yunganoside E2, glycyrrhizic acid) in Glycyrrhiza uralensis Fisch. roots. Validation of the procedure showed that the metrological parameters were satisfactory. The procedure was used for research on G. uralensis roots growing in Siberia and quantitative analysis of glycyrrhizic acid in 28 commercial licorice preparations.
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页码：986 / 991
页数：5
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