Iodocyclization of 2-[allyl(methallyl)sulfanyl]-6-(trifluoromethyl)pyrimidin-4(3H)-ones

被引：0
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作者：
T. V. Frolova
D. G. Kim
P. A. Slepukhin
机构：
[1] South Ural State University,Postovskii Institute of Organic Synthesis, Ural Branch
[2] Russian Academy of Sciences,undefined
来源：
Russian Journal of Organic Chemistry | 2016年 / 52卷
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摘要：
Iodination of 2-[allyl(methallyl)sulfanyl]-6-(trifluoromethyl)pyrimidin-4(3H)-ones was accompanied by cyclization to 2,3-dihydro[1,3]thiazolo[3,2-a]pyrimidin-4-ium triiodides. 3-(Iodomethyl)-3-methyl- 7-oxo-5-(trifluoromethyl)-2,3-dihydro[1,3]thiazolo[3,2-a]pyrimidin-4-ium triiodide was reduced with sodium iodide to 3,3-dimethyl-7-oxo-5-(trifluoromethyl)-2,3-dihydro[1,3]thiazolo[3,2-a]pyrimidin-4-ium iodide.
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页码：1344 / 1347
页数：3
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