Synthesis and characterization of ordered mesoporous silica containing di-ureasil hybrid/phosphotungstic acid and Eu3+

被引：0
|
作者：
C. T. Cavalcante
C. Molina
T. S. Martins
机构：
[1] Federal University of São Paulo (UNIFESP),Deparment of Chemistry
来源：
Journal of Materials Science: Materials in Electronics | 2019年 / 30卷
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摘要：
Multifunctional composite (MFC) di-ureasil hybrid synthesized by sol gel method containing phosphotungstic acid (PWA) and Eu3+ ions have been successfully incorporated into mesoporous silica (SBA-15) by post-synthesis method. MFC were characterized by Fourier transform-infrared spectroscopy (FTIR), small angle X-ray scattering (SAXS), nitrogen adsorption–desorption (NAI), thermogravimetric and differential thermal analysis, transmission electron microscopy (TEM) and also photoluminescence. FTIR showed that both di-ureasil and PWA were incorporated into the mesoporous silica. NAI, TEM and SAXS confirmed the incorporation of the PWA and di-ureasil into the mesoporous of SBA-15. Composites are thermal stable at about 240 °C and photoluminescence has demonstrated that Eu3+ ions were successfully entrapped and occupies local environment with low symmetry.
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页码：16903 / 16909
页数：6
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