Determination of Gaseous Formic and Acetic Acids by a Needle-Type Extraction Device coupled to a Gas Chromatography-Barrier Discharge Ionization Detector

被引:0
|
作者
Ikuo Ueta
Yohei Nakamura
Koji Fujimura
Susumu Kawakubo
Yoshihiro Saito
机构
[1] University of Yamanashi,Department of Applied Chemistry
[2] Shinwa Chemical Industries Ltd.,Department of Environmental and Life Sciences
[3] Toyohashi University of Technology,undefined
来源
Chromatographia | 2017年 / 80卷
关键词
Formic acid; Acetic acid; Needle-type extraction device; GC-BID;
D O I
暂无
中图分类号
学科分类号
摘要
Gaseous formic acid (FA) and acetic acid (AA) were concentrated by a needle-type extraction device, and the extracted analytes were determined using a gas chromatography-barrier discharge ionization detector. An activated carbon particle showed good extraction/desorption performance for FA and AA. The limit of quantification for FA and AA was 900 and 180 ng L−1 at sample volumes of 100 mL, and 150 and 30 ng L−1 at a sample volume of 600 mL, respectively. The storage performance of the analytes in the extraction needle was quantitatively evaluated at different temperatures, and the applicability of the proposed method to determine FA and AA in air samples was demonstrated.
引用
收藏
页码:151 / 156
页数:5
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