Mesoporous spheres of Dy2NiMnO6 synthesized via hydrothermal route for structural, morphological, and electrochemical investigation

被引:0
|
作者
Jashandeep Singh
Irina Rogge
Uttam Kumar Goutam
Ashok Kumar
机构
[1] National Institute of Technology Kurukshetra,Department of Physics
[2] Free University of Berlin,Department of Physics
[3] Bhabha Atomic Research Centre,Technical Physics Division
[4] National Institute of Technical Teachers Training and Research,Department of Applied Sciences
来源
Ionics | 2020年 / 26卷
关键词
Inorganic oxide materials; Double perovskite; Rare earth; Hydrothermal; Electrochemical;
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中图分类号
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摘要
Here, we report the synthesis of the double perovskite-mesoporous spheres of Dy2NiMnO6 via hydrothermal process exhibiting P21/n monoclinic symmetry. Field emission electron micrographs confirmed the formation of porous spheres. The elemental mapping exhibited the homogenous distribution of metal ions, i.e., Dy3+, Ni2+, and Mn3+/Mn4+ as observed via X-ray photoelectron spectroscopy. The Dy2NiMnO6 spheres exhibited a specific surface area of ~ 38 m2/g, with an average pore diameter of ~ 10 nm. The specific capacitance for mesoporous spheres of Dy2NiMnO6 has been found to be ~ 395.2 F/g at the scan rate of 0.5 A/g. Furthermore, mesoporous spheres of Dy2NiMnO6 displayed stability over 2500 cycles with 71% specific capacitance retention at constant current destiny of 3 A/g.
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页码:5143 / 5153
页数:10
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