Fully automated in-tube solid-phase microextraction for liquid samples coupled to gas chromatography

被引:0
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作者
Daniel Globig
Christian Weickhardt
机构
[1] Brandenburg University of Technology,Department of Physical and Analytical Chemistry
[2] Leipzig University of Applied Sciences,Department of Computer Science, Mathematics and Natural Sciences
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关键词
Solid-phase microextraction; In-tube SPME; Automation; Gas chromatography;
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摘要
An online device is described in which analytes are extracted from a liquid sample by means of in-tube solid-phase microextraction (in-tube SPME), pulse released by rapid heating, and transferred to a gas chromatograph in a fully automated way. Switching of the sample and gas flows as well as the heating of the extraction tube and the valves is controlled by a remote computer system. Results obtained for river water and for aqueous standard solutions of phenanthrene are presented and are compared to the performance of standard SPME.
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页码:656 / 659
页数:3
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