Synthesis and crystal structure of p-tert-butylcalix[4]arene 1,3-distal and monosubstituted semicarbazones and thiosemicarbazones

被引：0

作者：

Zhenming Liu

Dongmei Liu

Jinxiang Wang

Jing Sun

Chaoguo Yan

机构：

[1] Yangzhou University,Analysis and Test Center

[2] Yangzhou University,College of Chemistry & Chemical Engineering

来源：

Chemical Research in Chinese Universities | 2014年 / 30卷

关键词：

Calixarene; Semicarbazide; Semicarbazone; Thiosemicarbazone; Schiff base; Crystal structure;

D O I：

暂无

中图分类号：

学科分类号：

摘要：

A series of p-tert-butylcalix[4]arene 1,3-distal and monosubstituted semicarbazones and thiosemicarbazones was preparedd by acid catalyzed condensation reaction of active calixarene aldehydes with semicarbazide and thiocarbazide in methanol. One representative single crystal was determined by X-ray dirraction method, which shows that calixarene exists in cone configuration and intramolecular hydrogen-bands exist in the crystal.

引用

页码：415 / 419

页数：4

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