The aim of this study was to develop the methodology for collection and analysis of radon from a natural gas pipeline. Activated charcoal was used as collection media. Two methods were designed for collecting radon gas samples from onshore and offshore production sites. For onshore sites a continuous gas sampling method from the pipeline was developed. In case of offshore sites, a batch sampling method was designed. Gamma spectroscopy was utilized to determine the concentration of radon by analysis of radon daughters on the charcoal.