Microwave assisted synthesis of Thiacalix[n]arenes

被引：0
|
作者：
Mitesh H. Patel
Pranav S. Shrivastav
机构：
[1] Gujarat University,Chemistry Department, School of Sciences
来源：
Journal of Inclusion Phenomena and Macrocyclic Chemistry | 2009年 / 63卷
关键词：
Microwave; Thiacalixarenes; LC-MS; TC7A; Oligomers;
D O I：
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学科分类号：
摘要：
As a part of our ongoing investigations to unfold the chemistry of thiacalixarenes, this communication presents microwave assisted synthesis of thiacalix[n]arene macrocycles. This methodology entails combination of conventional heating and microwave irradiation to synthesize the entire series of thiacalix[n]arene analogs (n = 4, 5, 6, 7 and 8) with optimal yields and reaction time. LC-MS was used to monitor the progress/outcome of such reactions.
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页码：379 / 382
页数：3
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