Synthesis, Characterization and Thermal Decomposition of M1[M2(C2O4)2]xH2O (x=5 for M1=Co and x=4 for M1=Cd; M2=Ni)

被引：0
|
作者：
N. Deb
S. D. Baruah
N. N. Dass
机构：
[1] North Eastern Regional Institute of Science and Technology,Department of Chemistry
[2] Nirjuli,Department of Chemistry
[3] Regional Research Laboratory,undefined
[4] Jorhat,undefined
[5] Dibrugarh University,undefined
[6] Dibrugarh,undefined
来源：
Journal of Thermal Analysis and Calorimetry | 2000年 / 59卷
关键词：
IR; oxalato complexes; thermal decomposition;
D O I：
暂无
中图分类号：
学科分类号：
摘要：
Cobalt bis(oxalato)nickelate pentahydrate, Co[Ni(C2O4)2]5H2O and cadmium bis(oxalato)nickelate tetrahydrate, Cd[Ni(C2O4)2]4H2O have been synthesized and characterized by elemental analysis, reflectance and IR spectral studies. Thermal decomposition studies (TG, DTG and DTA ) in air showed that both the compound of cobalt and cadmium produced the oxide, MNiOx (x=3 for M=Co; x=2 for M=Cd ) at 325 and 360°C respectively. DSC studies in nitrogen attributed only the mixture of both the metal at the end.
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页码：791 / 797
页数：6
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