1,7-dithioxo systems. Reaction of 3-[(5,5-dimethyl-3-thioxocyclohex-1-en-1yl)sulfanyl]-5,5-dimethylcyclohex-2-ene-1-thione with 2-aminoethanol and ethane-1,2-diamine

被引：0
|
作者：
L. V. Timokhina
L. V. Kanitskaya
机构：
[1] Russian Academy of Sciences,Favorskii Irkutsk Institute of Chemistry, Siberian Division
来源：
Russian Journal of Organic Chemistry | 2009年 / 45卷
关键词：
Hydrogen Sulfide; Vinyl Ether; Sulfanyl; Anhydrous Acetonitrile; Hexahydro;
D O I：
暂无
中图分类号：
学科分类号：
摘要：
The reaction of 3-[(5,5-dimethyl-3-thioxocyclohex-1-en-1-yl)sulfanyl]-5,5-dimethylcyclohex-2-ene-1-thione with 2-aminoethanol involves cleavage of the sulfide bond with formation of 3-[(2-hydroxyethyl)-amino]-5,5-dimethylcyclohex-2-ene-1-thione as the major product. The reaction of the same sulfide with ethane-1,2-diamine gave previously unknown 3-({2-[(5,5-dimethyl-3-thioxocyclohex-1-en-1-yl)amino]ethyl}-amino)-5,5-dimethylcyclohex-2-ene-1-thione.
引用
收藏
页码：1795 / 1798
页数：3
相关论文
共 50 条
  • [1] 1,7-dithioxo systems. Reaction of 3-[(5,5-dimethyl-3-thioxocyclohex-1-en-1yl)sulfanyl]-5,5-dimethylcyclohex-2-ene-1-thione with 2-aminoethanol and ethane-1,2-diamine
    Timokhina, L. V.
    Kanitskaya, L. V.
    RUSSIAN JOURNAL OF ORGANIC CHEMISTRY, 2009, 45 (12) : 1795 - 1798
  • [2] 1,7-dithioxo systems. Reaction of bis(5,5-dimethyl-3-thioxocyclohex-1-en-1-yl) sulfide with amines
    Timokhina, L. V.
    Sokol'nikova, O. V.
    Kanitskaya, L. V.
    Yashchenko, M. P.
    Voronkov, M. G.
    RUSSIAN JOURNAL OF ORGANIC CHEMISTRY, 2008, 44 (04) : 532 - 535
  • [3] 1,7-Dithioxo systems. Reaction of bis(5,5-dimethyl-3-thioxo-cyclohex-1-en-1-yl) sulfide with amines
    L. V. Timokhina
    O. V. Sokol’nikova
    L. V. Kanitskaya
    M. P. Yashchenko
    M. G. Voronkov
    Russian Journal of Organic Chemistry, 2008, 44 : 532 - 535
  • [4] 1,7-dithioxo systems. Synthetic routes to bis(5,5-dimethyl-3-thioxo-1-cyclohexenyl) sulflde
    Timokhina, LV
    Panova, GM
    Kanitskaya, LV
    Sokol'nikova, OV
    Toryashinova, DSD
    Voronkov, MG
    RUSSIAN JOURNAL OF ORGANIC CHEMISTRY, 2001, 37 (11) : 1655 - 1658
  • [5] 1,7-Dithioxo Systems. Synthetic Routes to Bis(5,5-dimethyl-3-thioxo-1-cyclohexenyl) Sulfide
    L. V. Timokhina
    G. M. Panova
    L. V. Kanitskaya
    O. V. Sokol'nikova
    D. -S. D. Toryashinova
    M. G. Voronkov
    Russian Journal of Organic Chemistry, 2001, 37 : 1655 - 1658
  • [6] 1,7-Dithioxo-substituted systems. Bis(5,5-dimethyl-3-thioxocyclohex-1-enyl) sulfide in reactions with metals
    Timokhina, L. V.
    Sokol'nikova, O. V.
    Kanitskaya, L. V.
    Fedorov, S. V.
    Toryashinova, D.-S. D.
    Yashchenko, M. P.
    Voronkov, M. G.
    RUSSIAN JOURNAL OF GENERAL CHEMISTRY, 2007, 77 (08) : 1342 - 1345
  • [7] 1,7-Dithioxo-substituted systems. Bis(5,5-dimethyl-3-thioxocyclohex-1-enyl) sulfide in reactions with metals
    L. V. Timokhina
    O. V. Sokol’nikova
    L. V. Kanitskaya
    S. V. Fedorov
    D. -S. D. Toryashinova
    M. P. Yashchenko
    M. G. Voronkov
    Russian Journal of General Chemistry, 2007, 77 : 1342 - 1345
  • [8] 1,7-dithioxo systems. Photochemical, thermal, and chemical stabilities of bis(5,5-dimethyl-3-thioxo-1-cyclohexenyl) sulfide
    Timokhina, LV
    Panova, GM
    Kanitskaya, LV
    Sokol'nikova, OV
    Voronkov, MG
    RUSSIAN JOURNAL OF GENERAL CHEMISTRY, 2004, 74 (10) : 1569 - 1571
  • [9] 1,7-Dithioxo systems. Photochemical, thermal, and chemical stabilities of bis(5,5-dimethyl-3-thioxo-1-cyclohexenyl) sulfide
    L. V. Timokhina
    G. M. Panova
    L. V. Kanitskaya
    O. V. Sokol’nikova
    M. G. Voronkov
    Russian Journal of General Chemistry, 2004, 74 : 1569 - 1571
  • [10] N,N-′bis(5,5-dimethyl-2-thioxo-1,3,2-dioxaphosphinan-2-yl)ethane-1,2-diamine
    Li, Hai-Bing
    Li, Ya
    Xiong, De-Jun
    Tian, De-Mei
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2007, 63 : O606 - O607
12345