Microstructure and intergranular diffusion in exchange-coupled Sm-Co/Fe nanocomposites
被引:37
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作者:
Zhang, Ying
论文数: 0引用数: 0
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机构:
US DOE, Ames Lab, Mat Sci & Engn, Ames, IA 50011 USA
Univ Texas Arlington, Dept Phys, Arlington, TX 76019 USAUS DOE, Ames Lab, Mat Sci & Engn, Ames, IA 50011 USA
Zhang, Ying
[1
,2
]
Kramer, M. J.
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h-index: 0
机构:
US DOE, Ames Lab, Mat Sci & Engn, Ames, IA 50011 USAUS DOE, Ames Lab, Mat Sci & Engn, Ames, IA 50011 USA
Kramer, M. J.
[1
]
Rong, Chuanbing
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h-index: 0
机构:
Univ Texas Arlington, Dept Phys, Arlington, TX 76019 USAUS DOE, Ames Lab, Mat Sci & Engn, Ames, IA 50011 USA
Rong, Chuanbing
[2
]
Liu, J. Ping
论文数: 0引用数: 0
h-index: 0
机构:
Univ Texas Arlington, Dept Phys, Arlington, TX 76019 USAUS DOE, Ames Lab, Mat Sci & Engn, Ames, IA 50011 USA
Liu, J. Ping
[2
]
机构:
[1] US DOE, Ames Lab, Mat Sci & Engn, Ames, IA 50011 USA
[2] Univ Texas Arlington, Dept Phys, Arlington, TX 76019 USA
annealing;
cobalt alloys;
diffusion;
electron energy loss spectra;
exchange interactions (electron);
iron alloys;
nanocomposites;
nanomagnetics;
samarium alloys;
transmission electron microscopy;
PERMANENT-MAGNETS;
ENERGY PRODUCT;
CO;
D O I:
10.1063/1.3467202
中图分类号:
O59 [应用物理学];
学科分类号:
摘要:
We demonstrate homogenous distribution of bcc FeCo soft phase with grain size of 20-30 nm in the annealed Sm-Co/Fe bulk samples by energy filtered transmission electron microscopy (EFTEM). Quantitative Co/Fe interdiffusion measured using both energy dispersive spectroscopy (EDS) and parallel electron energy loss spectroscopy (PEELS) shows Fe60 +/- 5%Co40 +/- 5% for the magnetically soft bcc phase and Sm-2(Co0.82Fe0.18)(7) and Sm(Co0.80Fe0.20)(5) respectively for the magnetically hard phases in these two alloy systems after optimal annealing. The graded interface develops in both samples due to the Co/Fe interchange between the hard and soft phases and the bcc soft phase was determined. (C) 2010 American Institute of Physics. [doi: 10.1063/1.3467202]