Fabrication and magnetic properties of NiFe2O4 nanorods

NiFe2O4 nanorods have been successfully synthesized via thermal treatment of the rod-like precursor fabricated by Ni-doped alpha-FeOOH, which was enwrapped by the complex of citric acid and Ni2+. The morphology evolution during the calcination of the precursor nanorods was investigated with transmission electron microscopy (TEM), and the phase and the magnetic properties of samples were analyzed through X-ray diffraction (XRD) and vibrating sample magnetometer (VSM). The results indicated that the diameter of the NiFe2O4 nanorods obtained ranged between 30 and 50 nm, and the length ranged between 2 and 3 pm. As the calcination temperature was up to 600 degrees C, the coercivity, saturation magnetization, and remanent magnetization of the samples were 36.1 kA.m(-1), 27.2 A-m(2).kg(-1), and 5.3 A.m(2).kg(-1), respectively. The NiFe2O4 nanorods prepared have higher shape anisotropy and superior magnetic properties than those with irregular shapes.