10-[2-(4-Acetylpiperzin-1-yl)ethyl]-9-(4-chlorophenyl)-3,3,6,6-tetramethyl-3,4,6,7,9,10-hexahydro-2H,5H-acridine-1,8-dione

被引:0
|
作者
Seshadri, PR
Yogavel, M
Rajan, TJ
Velmurugan, D
Raj, SSS
Fun, HK
机构
[1] Univ Madras, Dept Crystallog & Biophys, Madras 600025, Tamil Nadu, India
[2] Univ Madras, Dept Organ Chem, Madras 600025, Tamil Nadu, India
[3] Univ Sains Malaysia, Sch Phys, George Town 11800, Malaysia
[4] Agurchand Manmull Jain Coll, Dept Phys, Madras 600114, Tamil Nadu, India
关键词
D O I
10.1107/S1600536803007530
中图分类号
O7 [晶体学];
学科分类号
0702 ; 070205 ; 0703 ; 080501 ;
摘要
In the title compound, C31H40N3O3Cl, the central N-containing ring adopts a boat conformation and the two outer rings adopt conformations intermediate between half-chair and sofa. In the crystal structure, C-H...O hydrogen bonds link the symmetry-related molecules to form centrosymmetric hydrogen-bonded tetramers with R-4(4)(24) and R-4(4)(52) motifs.
引用
收藏
页码:O696 / O698
页数:3
相关论文
共 50 条
  • [1] Synthesis and crystal structures of 3,3,6,6-tetramethyl-9-(2,4-dichlorophenyl)-3,4,6,7,9,10-hexahydro-2H,5H-acridine-1,8-dione and 3,3,6,6-tetramethyl-9,10-di(4-methoxyphenyl)-3,4,6,7,9,10-hexahydro-2H,5H-acridine-1,8-dione
    Shi, Da-Qing
    Ni, Sai-Nan
    Yang, Fang
    Li, Xiao-Yue
    Wang, Xiang-Shan
    JOURNAL OF CHEMICAL CRYSTALLOGRAPHY, 2007, 37 (07) : 483 - 487
  • [2] Synthesis and Crystal Structures of 3,3,6,6-tetramethyl-9-(2,4-dichlorophenyl)-3,4,6,7,9,10-hexahydro-2H,5H-acridine-1,8-dione and 3,3,6,6-tetramethyl-9,10-di(4-methoxyphenyl)-3,4,6,7,9,10-hexahydro-2H,5H-acridine-1,8-dione
    Da-Qing Shi
    Sai-Nan Ni
    Fang Yang
    Xiao-Yue Li
    Xiang-Shan Wang
    Journal of Chemical Crystallography, 2007, 37 : 483 - 487
  • [3] 10-(4-chlorophenyl)-9-(4-fluorophenyl)-3,3,6,6-tetramethyl-3,4,6,7,9,10-hexahydroacridine-1,8(2H,5H)-dione
    Zhao, Ling-Ling
    Teng, Da
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2008, 64 : O1772 - U2091
  • [4] 9-(4-Dimethylaminophenyl)-3,3,6,6-tetramethyl-3,4,6,7,9,10-hexahydro-1,8(2H,5H)-acridinedione
    Ganesh, VK
    Velmurugan, D
    Sagar, MB
    Murugan, P
    ACTA CRYSTALLOGRAPHICA SECTION C-CRYSTAL STRUCTURE COMMUNICATIONS, 1998, 54 : 557 - 559
  • [5] 9-(2,4-Difluorophenyl)-3,3,6,6-tetramethyl-3,4,5,6,7,9-hexahydro-2H-xanthene-1,8-dione
    Begum, S. Rizwana
    Hema, R.
    Sumathi, G.
    Valliappan, R.
    Srinivasan, N.
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2014, 70 : O276 - +
  • [6] 9-(4-chlorophenyl)-3,3,6,6-tetramethyl-1,2,3,4,5,6,7,8,9,10-decahydroacridine-1,8-dione
    Tu, SJ
    Deng, X
    Du, M
    Fang, YY
    Guo, YM
    Liu, XH
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2001, 57 : O383 - O385
  • [7] 10-(4-Chlorophenyl)-9-(4-methoxyphenyl)3,3,6,6-tetramethyl-3,4,6,7-tetrahydroacridine-1,8(2H,5H,9H,10H)-dione
    Chen, Yan
    Hao, Wen-Juan
    Tang, Zi-Qiang
    Jiang, Bo
    Li, Chun-Mei
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2007, 63 : O3934 - U1926
  • [8] 10-[2-(Dimethylamino)ethyl]-9-(4-methoxyphenyl)-3,3,6,6-tetramethyl)-3,4,6,7,9,10-hexahydroacridine-1,8(2H,5H)-dione
    Balamurugan, P.
    Jagan, R.
    Thiagarajan, V.
    Yamin, Bohari M.
    Sivakumar, K.
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2009, 65 : O271 - U1699
  • [9] 9-(1,3-benzodioxol-5-yl)-10-(4-chlorophenyl)-3,3,6,6-tetramethyl-3,4,6,7-tetrahydroacridine-1,8(2H,5H,9H,10H)-dione
    Quande Liu
    Ziqiang Tang
    Xihua Du
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2007, 63 : O3924 - U4087
  • [10] 9-(4-chlorophenyl)-3,3,6,6-tetramethyl-10-(4-methylphenyl)-1,2,3,4,5,6,7,8,9,10-decahydroacridine-1,8-dione
    Wang, XS
    Shi, DQ
    Tu, SJ
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2003, 59 : O1139 - O1140