Exploration of crystal strains using coherent x-ray diffraction

被引:27
|
作者
Cha, Wonsuk [1 ]
Song, Sanghoon [2 ]
Jeong, Nak Cheon [3 ]
Harder, Ross [4 ]
Yoon, Kyung Byung [2 ,3 ]
Robinson, Ian K. [5 ,6 ]
Kim, Hyunjung [1 ,2 ]
机构
[1] Sogang Univ, Dept Phys, Seoul 121742, South Korea
[2] Sogang Univ, Interdisciplinary Program Integrated Biotechnol, Seoul 121742, South Korea
[3] Sogang Univ, Dept Chem, Seoul 121742, South Korea
[4] Argonne Natl Lab, Adv Photon Source, Argonne, IL 60439 USA
[5] UCL, Dept Phys & Astron, London WC1H 0AH, England
[6] Diamond Light Source, Didcot OX11 0DE, Oxon, England
来源
NEW JOURNAL OF PHYSICS | 2010年 / 12卷
基金
英国工程与自然科学研究理事会;
关键词
ZEOLITE; ARRAYS; ZSM-5;
D O I
10.1088/1367-2630/12/3/035022
中图分类号
O4 [物理学];
学科分类号
0702 ;
摘要
We measured coherent x-ray diffraction (CXD) on zeolite microcrystals in order to gain information on internal density distribution and to learn more about the strain developed during the synthesis and attachment process on the substrate. From the distortion and asymmetry of the diffraction pattern on the (020) Bragg peak, the strain field distribution is estimated. We inverted the diffraction patterns from a less strained crystal to obtain the three-dimensional image of the shape and internal strain fields using the error reduction and hybrid input-output phase retrieval algorithms. We also show a few examples of characteristic distortion modes relevant to CXD of zeolites.
引用
收藏
页数:10
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