Antibacterial activity of silver nanoparticles synthesized from serine

被引:43
|
作者
Jayaprakash, N. [1 ,2 ]
Vijaya, J. Judith [1 ]
Kennedy, L. John [3 ]
Priadharsini, K. [4 ]
Palani, P. [4 ]
机构
[1] Loyola Coll, Dept Chem, Catalysis & Nanomat Res Lab, Madras 600034, Tamil Nadu, India
[2] SRM Valliammai Engn Coll, Dept Chem, Madras 603203, Tamil Nadu, India
[3] VIT Univ, Sch Adv Sci, Div Mat, Madras 600048, Tamil Nadu, India
[4] Univ Madras, Dept Ctr Adv Study Bot, Madras 600025, Tamil Nadu, India
关键词
Silver nanoparticles; Serine; Photoluminescence; Electron microscopy; Microwave irradiation; DL-SERINE; GOLD; POLYMER; ACID; SURFACTANTS; ABSORPTION; CHEMISTRY; GROWTH; SHAPE; SIZE;
D O I
10.1016/j.msec.2015.01.012
中图分类号
TB3 [工程材料学]; R318.08 [生物材料学];
学科分类号
0805 ; 080501 ; 080502 ;
摘要
Silver nanoparticles (Ag NPs) were synthesized by a simple microwave irradiation method using polyvinyl pyrrolidone (PVP) as a capping agent and serine as a reducing agent. UV-Visible spectra were used to confirm the formation of Ag NPs by observing the surface plasmon resonance (SPR) band at 443 nm. The emission spectrum of Ag NPs showed an emission band at 484 nm. In the presence of microwave radiation, serine acts as a reducing agent, which was confirmed by Fourier transformed infrared (FT-IR) spectrum. High-resolution transmission electron microscopy (HR-TEM) and high-resolution scanning electron microscopy (HR-SEM) were used to investigate the morphology of the synthesized sample. These images showed the sphere-like morphology. The elemental composition of the sample was determined by the energy dispersive X-ray analysis (EDX). Selected area electron diffraction (SAED) was used to find the crystalline nature of the Ag NPs. The electrochemical behavior of the synthesized Ag NPs was analyzed by the cyclic voltammetry (CV). Antibacterial experiments showed that the prepared Ag NPs showed relatively similar antibacterial activities, when compared with AgNO3 against Gram-positive and Gram-negative bacteria. (C) 2015 Elsevier B.V. All rights reserved.
引用
收藏
页码:316 / 322
页数:7
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