Synthesis and characterization of antimony tartrate for ceramic precursors

被引：6

作者：

Mazali, IO ^{[1
]}

Las, WC ^{[1
]}

Cilense, M ^{[1
]}

机构：

[1] UNESP, Inst Quim, Dept Fisicoquim, BR-14801970 Araraquara, SP, Brazil

来源：

JOURNAL OF MATERIALS SYNTHESIS AND PROCESSING | 1999年 / 7卷 / 06期

关键词：

Pechini's method; chemical synthesis; antimony tartrate; characterization; ceramic precursor;

D O I：

10.1023/A:1021822115116

中图分类号：

T [工业技术];

学科分类号：

08 ;

摘要：

Synthesis and characterization of antimony tartrate used as a precursor of ceramic powders obtained by Pechini's method were carried out. Antimony tartrate was chosen as a substitute for the antimony citrate commonly used in this chemical processing, because of difficulties in preparing the citrate. FTIR and TGA/DTA analysis showed that antimony tartrate, H-2[Sb-2(C4H2O6)(2)]. forms a polymeric structure. The procedure described indicates that the antimony chelate obtained is adequate for Pechini's method.

引用

页码：387 / 391

页数：5

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