Study on Determination of Polyphenols in Tobacco by Gas Chromatography-Mass Spectrometry

被引：0
|
作者：
Shi, Hong-Lin [1 ]
Xu, Yi-Ran [1 ]
Miao, Ming-Ming [1 ]
Yang, Guang-Yu [1 ]
Hu, Qiu-Fen [1 ]
机构：
[1] Yunnan Inst Nationalities, Dept Chem, Kunming 650031, Peoples R China
来源：
ASIAN JOURNAL OF CHEMISTRY | 2010年 / 22卷 / 02期
关键词：
Gas-MS; Polyphenols; Derivatization; Tobacco;
D O I：
暂无
中图分类号：
O6 [化学];
学科分类号：
0703 ;
摘要：
A gas chromatography-mass spectrometry method for the determination of polyphenols (chlorogenic acid, rutin and scopoletin) in tobacco samples was studied. The polyphenols were extracted from the samples by ultrasonic extraction and a 99:1 mixture of N,O-bis(trimethylsilyl)trifluoroacetamide and trimethylchlorosilane was used for derivatization. With GC-MS detection in single-ion-monitoring mode, the main polyphenols (chlorogenic acid, rutin and scopoletin) were analyzed quantitatively. The limit of detections (S/N = 3) were below 50 ng/mL, the relative standard deviations (RSD) were below 3.2 % (n = 7) and the recoveries were in the range of 92-106 %.
引用
收藏
页码：1192 / 1196
页数：5
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