Synthesis of nano-powder materials using spray-pyrolysis method

被引:2
|
作者
Gornicka, Barbara [1 ]
Mazurek, Boleslaw [1 ]
Mielcarek, Witold [1 ]
Prociow, Krystyna [1 ]
Warycha, Joanna [1 ]
机构
[1] Electrotech Inst, Div Electrotechnol & Mat Sci, Ul M Sklodowskiej Curie 55-61, PL-50369 Wroclaw, Poland
关键词
nano-size crystallite zinc oxide; spray pyrolysis; methane sensor;
D O I
10.4028/www.scientific.net/SSP.128.13
中图分类号
TB3 [工程材料学];
学科分类号
0805 ; 080502 ;
摘要
In this work the laboratory-scale installation for synthesising powder materials with nano-size grains is presented. Nano-sized zinc and tin oxides were obtained using the spray-pyrolysis (SP) method. The zinc oxide was derived from zinc acetate at 300 degrees C, 430 degrees C, 580 degrees C, 800 degrees C and 950 degrees C. The tin oxide was processed by the thermal decomposition of tin tartrate at 500 degrees C. The SP synthesized zinc oxide was used for manufacturing a methane sensor which was characterized as possessing a much wider range of operating and substantially higher sensitivity, 10 times higher. to methane gas compared to a sensor made out of commercially available zinc oxide.
引用
收藏
页码:13 / +
页数:2
相关论文
共 50 条
  • [1] CERAMIC POWDER SYNTHESIS BY SPRAY-PYROLYSIS
    MESSING, GL
    ZHANG, SC
    JAYANTHI, GV
    [J]. JOURNAL OF THE AMERICAN CERAMIC SOCIETY, 1993, 76 (11) : 2707 - 2726
  • [2] SYNTHESIS OF CATALYTIC MATERIALS BY SPRAY-PYROLYSIS
    WOLD, A
    MILLER, D
    KERSHAW, R
    [J]. ABSTRACTS OF PAPERS OF THE AMERICAN CHEMICAL SOCIETY, 1995, 209 : 38 - PETR
  • [3] CHARACTERISATION OF NANO-POWDER MORPHOLOGY OBTAINED BY ULTRASONIC SPRAY PYROLYSIS
    Stopic, Srecko
    Friedrich, Bernd
    Raic, Karlo
    Volkov-Husovic, Tatjana
    Dimitrijevic, Marija
    [J]. METALLURGICAL & MATERIALS ENGINEERING-ASSOCIATION OF METALLURGICAL ENGINEERS OF SERBIA, 2008, 14 (01): : 41 - 54
  • [4] SIMULATION OF SPRAY-PYROLYSIS FOR CERAMIC POWDER PREPARATION
    YU, HF
    [J]. PARTICULATE SCIENCE AND TECHNOLOGY, 1995, 13 (02) : 149 - 167
  • [5] Synthesis of carbon nanotubes from liquid hydrocarbons using a spray-pyrolysis method
    Faculty of Physics, Babeş-Bolyai University, Kogalniceanu 1, Cluj-Napoca, 400084, Romania
    不详
    不详
    不详
    [J]. J. Optoelectron. Adv. Mat., 2008, 9 (2307-2310):
  • [6] Synthesis of carbon nanotubes from liquid hydrocarbons using a spray-pyrolysis method
    Sarkoezi, Zs.
    Kertesz, K.
    Koos, A. A.
    Osvath, Z.
    Tapaszto, L.
    Horvath, Z. E.
    Nemes-Incze, P.
    Jenei, I. Z.
    Vertesy, Z.
    Daroczi, N. S.
    Darabont, Al.
    Pana, O.
    Biro, L. P.
    [J]. JOURNAL OF OPTOELECTRONICS AND ADVANCED MATERIALS, 2008, 10 (09): : 2307 - 2310
  • [7] Synthesis of ZnO Nanoparticles by Spray-Pyrolysis Method and Their Photocatalytic Effect
    Lee, Sang Duck
    Nam, Sang-Hun
    Kim, Myoung-Hwa
    Kim, Young Dok
    Boo, Jin-Hyo
    [J]. INEC: 2010 3RD INTERNATIONAL NANOELECTRONICS CONFERENCE, VOLS 1 AND 2, 2010, : 572 - 573
  • [8] Mechanochemical synthesis of nano-powder
    Ding, J
    Miao, WF
    Tsuzuki, T
    McCormick, PG
    Street, R
    [J]. SYNTHESIS AND PROCESSING OF NANOCRYSTALLINE POWDER, 1996, : 69 - 79
  • [9] Elaboration of boehmite nano-powders by spray-pyrolysis
    Caiut, J. M. A.
    Dexpert-Ghys, J.
    Kihn, Y.
    Verelst, M.
    Dexpert, H.
    Ribeiro, S. J. L.
    Messaddeq, Y.
    [J]. POWDER TECHNOLOGY, 2009, 190 (1-2) : 95 - 98
  • [10] Synthesis and Photocatalytic Property of ZnO nanoparticles Prepared by Spray-Pyrolysis Method
    Lee, Sang Duck
    Nam, Sang-Hun
    Kim, Myoung-Hwa
    Boo, Jin-Hyo
    [J]. 18TH INTERNATIONAL VACUUM CONGRESS (IVC-18), 2012, 32 : 320 - 326