2,2′-[1,2-phenylenebis(methylenethio)]bis(5-methyl-1,3,4-thiadiazole)

被引：6
|
作者：
Zheng, Y [1 ]
Liu, HB
机构：
[1] Tianjin Univ, Dept Chem, Tianjin 300072, Peoples R China
[2] Natl Res Ctr Testing Tech Bldg Mat, Beijing 100024, Peoples R China
来源：
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE | 2003年 / 59卷
关键词：
D O I：
10.1107/S1600536802021761
中图分类号：
O7 [晶体学];
学科分类号：
0702 ; 070205 ; 0703 ; 080501 ;
摘要：
The title compound (PBT), C14H14N4S4, possesses C-2 symmetry, with the twofold axis bisecting the central benzene ring. The two terminal 2-(5-methyl-1,3,4-thiodiazolyl)thio groups adopt a trans conformation with respect to the benzene moiety, and the dihedral angle between the two thiodiazole planes is 61.3 (2)degrees, while that between the thiodiazole and benzene planes is 79.4 (5)degrees.
引用
收藏
页码：O34 / O35
页数：2
相关论文
共 50 条
  • [1] catena-Poly[[(nitrato-κ2O,O′)-silver(I)]-μ-2,2′-[1,4-phenylenebis(methylenethio)]bis(5-methyl-1,3,4-thiadiazole)-κ2N3:N3′]
    Zheng, Y
    ACTA CRYSTALLOGRAPHICA SECTION C-STRUCTURAL CHEMISTRY, 2004, 60 : M471 - M472
  • [2] 2,2′-[1,2-phenylenebis(nitrilomethylidyne)]-bis(5-methylphenol)
    Eltayeb, Naser Eltaher
    Teoh, Siang Guan
    Teh, Jeannie Bee-Jan
    Fun, Hoong-Kun
    Ibrahim, Kamarulazizi
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2007, 63 : O695 - O696
  • [3] 2,2′-(1,4-butanediyldithio)bis(1,3,4-thiadiazole)
    Wang, Lu
    Zhang, Jun
    Ye, Bao-Xian
    Hu, Pu-Zhou
    Zhao, Bang-Tun
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2006, 62 : O4844 - O4846
  • [4] 2-Amino-5-methyl-1,3,4-thiadiazole and 2-amino-5-ethyl-1,3,4-thiadiazole
    Lynch, DE
    ACTA CRYSTALLOGRAPHICA SECTION C-STRUCTURAL CHEMISTRY, 2001, 57 : 1201 - 1203
  • [5] 2,2 '-[1,2-Phenylenebis(azanediyl)]diacetonitrile
    Rivera, Augusto
    Jimenez-Cruz, Leonardo
    Maldonado, Mauricio
    Kucerakova, Monika
    Dusek, Michal
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2012, 68 : O3429 - +
  • [6] STRUCTURE OF 2,2',5,5'-BIS(TETRAMETHYLENEDITHIO)DI-1,3,4-THIADIAZOLE
    CHO, SG
    FRONCZEK, FR
    TAYLOR, WS
    WATKINS, SF
    ACTA CRYSTALLOGRAPHICA SECTION C-CRYSTAL STRUCTURE COMMUNICATIONS, 1988, 44 : 769 - 771
  • [7] 5,5′-Dimethoxy-2,2′-[1,2-phenylenebis(nitrilomethylidyne)]diphenol
    Eltayeb, Naser Eltaher
    Teoh, Siang Guan
    Chantrapromma, Suchada
    Fun, Hoong-Kun
    Ibrahim, Kamarulazizi
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2007, 63 : O3094 - U2504
  • [8] 2-{[3-(4-chlorophenyl)-1,2,4-oxadiazol-5-yl]methylsulfanyl}-5-methyl-1,3,4-thiadiazole
    Wang, Pin-liang
    Li, Hai-ling
    Kang, Si-shun
    Wang, Hai-bo
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2007, 63 : O4411 - U4287
  • [9] Examining thermolysis reactions and tautomerism of 2-mercapto-5-methyl-1,3,4-thiadiazole and 2,5-dimercapto-1,3,4-thiadiazole
    Hipler, F
    Fischer, RA
    Müller, J
    JOURNAL OF THE CHEMICAL SOCIETY-PERKIN TRANSACTIONS 2, 2002, (09): : 1620 - 1626
  • [10] 1,3,4-thiadiazole derivatives .5. Heteropolynuclear complexes of 2-amino-5-mercapto-1,3,4-thiadiazole
    Brezeanu, M
    Olar, R
    Meghea, A
    Stanica, N
    Supuran, CT
    REVUE ROUMAINE DE CHIMIE, 1996, 41 (1-2) : 103 - 107
12345