The effect of titania precursor on the morphology of prepared TiO2/MWCNT nanocomposite materials

被引：6

作者：

Berki, Peter ^{[1
]}

Reti, Balazs ^{[1
]}

Terzi, Katerina ^{[2
]}

Bountas, Ioannis ^{[2
]}

Horvath, Endre ^{[3
]}

Fejes, Dora ^{[1
]}

Magrez, Arnaud ^{[2
]}

Tsakiroglu, Christos ^{[2
]}

Forro, Laszlo ^{[3
]}

Hernadi, Klara ^{[1
]}

机构：

[1] Univ Szeged, Dept Appl & Environm Chem, H-6720 Szeged, Hungary

[2] FORTH, Inst Chem Engn, Patras 26504, Greece

[3] Ecole Polytech Fed Lausanne, Lab Phys Complex Matter, CH-1015 Lausanne, Switzerland

来源：

PHYSICA STATUS SOLIDI B-BASIC SOLID STATE PHYSICS | 2014年 / 251卷 / 12期

关键词：

multiwalled carbon nanotubes; photocatalysis; slow hydrolysis; titanium dioxide; WALLED CARBON NANOTUBES; SOL-GEL METHOD; PHOTOCATALYTIC DEGRADATION; COMPOSITE; CATALYSTS; NANORODS; STRENGTH; COVERAGE; DIOXIDE; PHENOL;

D O I：

10.1002/pssb.201451161

中图分类号：

O469 [凝聚态物理学];

学科分类号：

070205 ;

摘要：

Since materials science is of great importance, the application of composite materials based on carbon nanotubes (CNTs) is widely investigated. Current work is aimed at preparing nanocomposites of TiO2/MWCNT using an impregnation method combined with slow hydrolysis. Different titanium alkoxide compounds as Ti(OEt)(4), Ti(OiPr)(4), and Ti(OBu)(4), respectively, were used as precursor materials to cover the surface of CNTs in ethanolic medium. In our samples themass ratiowas 10:1 (TiO2:MWCNT). The produced composite materials were characterized by X-ray diffraction (XRD), energy-dispersive X-ray spectroscopy (EDX), Raman microscopy, transmission (TEM) and scanning electron microscopy (SEM) techniques; moreover, thermal analysis and the determination of the specific surface area (BET) were also carried out. These as-prepared TiO2/MWCNT composites were also tested as photocatalysts in degradation reaction of the model compound salicylic acid. (C) 2014 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim

引用

页码：2384 / 2388

页数：5

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