Novel low-temperature synthesis of tin(0) nanoparticles

被引：22
|
作者：
Balan, L
Schneider, R
Billaud, D
Ghanbaja, J
机构：
[1] Univ Nancy 1, Lab Chim Solide Mineral, UMR 7555, F-54506 Vandoeuvre Les Nancy, France
[2] Univ Nancy 1, Lab Synth Organomet & Reactiv, UMR 7565, F-54506 Vandoeuvre Les Nancy, France
[3] Univ Nancy 1, Serv Commun Microscopie Elect Transmiss, F-54506 Vandoeuvre Les Nancy, France
来源：
MATERIALS LETTERS | 2005年 / 59卷 / 8-9期
关键词：
Sn(0) particles; synthesis; solution phase reduction; activated sodium hydride; nanomaterials;
D O I：
10.1016/j.matlet.2004.12.010
中图分类号：
T [工业技术];
学科分类号：
08 ;
摘要：
In this paper, we report a novel low-temperature solution phase reduction of SnCl2 with t-BuONa-activated NaH which affords colloidal Sn(0) nanoparticles with an average diameter of ca. 40 nm, The t-BuONa stabilized Sn(0) nanoparticles were characterized using X-ray powder diffraction, transmission electron microscopy, XPS, and EDS analyses. The influence of purification conditions on the aggregation state of Sn(0) particles is described. (C) 2004 Elsevier B.V. All rights reserved.
引用
收藏
页码：1080 / 1084
页数：5
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