Surface tension measurements of liquid metals by the quasi-containerless pendant drop method

被引:26
|
作者
Man, KF [1 ]
机构
[1] CALTECH, Jet Prop Lab, Pasadena, CA 91109 USA
基金
美国国家航空航天局;
关键词
digital image analysis; electron beam melting; high-temperature liquid metals; melting point; pendant drop; quasi-containerless; surface tension;
D O I
10.1023/A:1006601821432
中图分类号
O414.1 [热力学];
学科分类号
摘要
The surface tensions of liquid metals, Zr, Ni, Ti, Mo, and Nb, have been measured at their molting points using the quasi-containerless pendant drop method. This method involves melting the end of a high-purity metal rod by bombardment with an electron beam to form a pendant drop under ultrahigh-vacuum conditions to minimize surface contamination. The magnified image of the drop is captured from a high-resolution CCD camera and digitized using a frame-grabber, The digital image is analyzed by reading the pixel intensities from a graphics file. The edge coordinates of the drop along rows and columns of pixels art: searched by a computer program and stored in an array. An optimized theoretical drop shape is computed From the edge coordinates by solving the Young Laplace differential equation to deduce the surface tension. The measured surface tensions are compared with available experimental results and theoretical calculations.
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页码:793 / 804
页数:12
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