Preparation, phase constitution and ionic conductivity of nanophase PbF2

被引:0
|
作者
Liu, JF [1 ]
Wu, XJ
Xu, GL
Wang, PC
机构
[1] Zhejiang Univ, Dept Mat Sci & Engn, Hangzhou 310027, Peoples R China
[2] Chinese Acad Sci, Shanghai Inst Ceram, Shanghai 200050, Peoples R China
关键词
nanophase fluoride; phase transition; ionic conductivity;
D O I
暂无
中图分类号
TQ174 [陶瓷工业]; TB3 [工程材料学];
学科分类号
0805 ; 080502 ;
摘要
The bulk samples of nanophase PbF2(n-PbF2) with the clean interfaces were prepared by using an inert gas evaporation and in situ compacting technique. The phase constitution and ionic conductivity were studied by XRD, DSC and complex impedance spectra. The results show that the ionic conductivity of n-PbF2 is rather higher than that of coarse-grained PbF2. The temperature of phase transition from alpha-phase to beta-phase for n-PbF2 drops about 30 degrees C compared with that of coarse-grained PbF2.
引用
收藏
页码:447 / 450
页数:4
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