Facile sol-gel synthesis of reduced graphene oxide/silica nanocomposites

被引:28
|
作者
Hintze, Cornelia [1 ,4 ]
Morita, Koji [2 ]
Riedel, Ralf [1 ]
Ionescu, Emanuel [1 ,3 ]
Mera, Gabriela [1 ]
机构
[1] Tech Univ Darmstadt, Inst Mat Wissensch, Joyanka Bontschits Str 2, D-64287 Darmstadt, Germany
[2] Natl Inst Mat Sci, 1-2-1 Sengen, Tsukuba, Ibaraki 3050047, Japan
[3] Univ Cologne, Dept Chem, Inst Anorgan Chem, Greinstr 6, D-50939 Cologne, Germany
[4] Karlsruhe Inst Technol, Inst Festkorperphys, D-76121 Karlsruhe, Germany
关键词
Silica-graphene nanocomposites; Graphene; Sol-gel synthesis; Silicon oxycarbide; MECHANICAL-PROPERTIES; RAMAN-SPECTROSCOPY; OXIDE; SILICA; COMPOSITE; PHASE; GAS; TRANSPORT; CERAMICS; FILM;
D O I
10.1016/j.jeurceramsoc.2015.11.033
中图分类号
TQ174 [陶瓷工业]; TB3 [工程材料学];
学科分类号
0805 ; 080502 ;
摘要
Novel silica-containing nanocomposites with a controlled carbon phase based on high quality reduced graphene oxide (rGO) were prepared via a cheap and facile sol-gel method, followed by pyrolysis in inert gas atmosphere. The resulting nanocomposite materials have an intimate bonding between rGO of low defect density and a partially crystalline silica matrix, as shown by Raman, FTIR and HRTEM studies. This processing route allows a straight-forward control of the content of the carbon phase and an excellent dispersion thereof within the silica matrix. (C) 2015 Elsevier Ltd. All rights reserved.
引用
收藏
页码:2923 / 2930
页数:8
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