An efficient synthesis of pyridine containing triaza-macrocyclic triacetate ligand and luminescence properties of its europium(III) complex

被引：24
|
作者：
Siaugue, JM
Segat-Dioury, F
Favre-Réguillon, A
Madic, C
Foos, J
Guy, A
机构：
[1] Conservatoire Natl Arts & Metiers, Chim Organ Lab, CNRS, ESA 7084, F-75141 Paris 3, France
[2] Conservatoire Natl Arts & Metiers, Nucl Sci Lab, F-75003 Paris, France
[3] CEA Saclay, Direct Cycle Combustible, F-91191 Gif Sur Yvette, France
来源：
TETRAHEDRON LETTERS | 2000年 / 41卷 / 39期
关键词：
D O I：
10.1016/S0040-4039(00)01272-7
中图分类号：
O62 [有机化学];
学科分类号：
070303 ; 081704 ;
摘要：
Reaction of diethylenetriamine with 2-nitrobenzenesulfonyl chloride leads to an activated and protected compound that could be cyclized to N-protected aza-macrocycle. After a smooth deprotection step, the macrocycle was alkylated with chloroacetic acid leading to the pyridine containing triaza-macrocycle 1 in good yield. The luminescence properties of its Eu3+ complex were examined in aqueous solution. (C) 2000 Elsevier Science Ltd. All rights reserved.
引用
收藏
页码：7443 / 7446
页数：4
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