Alternative synthesis and crystal structure of a [2]boraferrocenophane

被引：24
|
作者：
Braunschweig, Holger [1 ]
Seeler, Fabian [1 ]
Sigritz, Rainer [1 ]
机构：
[1] Univ Wurzburg, Inst Anorgan Chem, D-97074 Wurzburg, Germany
来源：
JOURNAL OF ORGANOMETALLIC CHEMISTRY | 2007年 / 692卷 / 11期
关键词：
boron; iron; diborane(4); ansa-complexes;
D O I：
10.1016/j.jorganchem.2007.02.008
中图分类号：
O61 [无机化学];
学科分类号：
070301 ; 081704 ;
摘要：
The [2]boraferrocenophane [(eta(5) -C5H4)-B(NMe2)-B(NMe2)-(eta(5)-(CH4)-H-5)Fe] (1) was obtained from the reaction of FeCl2 and (Me2N)(2)B-2(eta(1)-C5H5)(2) as a diborane(4) based ligand precursor in very good yields and fully characterized in the solid by single crystal X-ray diffraction. (C) 2007 Elsevier B.V. All rights reserved.
引用
收藏
页码：2354 / 2356
页数：3
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