Apigenin-7-O-β-D-glycoside isolation from the highly copper-tolerant plant Elsholtzia splendens

被引：20
|
作者：
Peng, Hong-yun [1 ]
Zhang, Xue-hong [1 ]
Xu, Jin-zhong [2 ]
机构：
[1] Zhejiang Univ, Coll Environm & Resource Sci, Minist Educ, Key Lab Environm Remediat & Ecol Hlth, Hangzhou 310058, Zhejiang, Peoples R China
[2] Zhejiang Univ, Inst Marine Biol, Ocean Coll, Hangzhou 310058, Zhejiang, Peoples R China
来源：
JOURNAL OF ZHEJIANG UNIVERSITY-SCIENCE B | 2016年 / 17卷 / 06期
基金：
中国国家自然科学基金;
关键词：
Chromatographic separation; Copper-tolerant plant; Elsholtzia splendens; Flavonoid glycoside; Structure elucidation; ANTIOXIDATIVE CHARACTERISTICS; EXTRACTS; APIGENIN; GLYCOSIDES; MICE;
D O I：
10.1631/jzus.B1500242
中图分类号：
Q5 [生物化学]; Q7 [分子生物学];
学科分类号：
071010 ; 081704 ;
摘要：
Elsholtzia splendens (Lamiaceae) is a copper-tolerant plant species growing on copper deposits in the south of China. Chromatographic separation of n-BuOH extracts from the flowering aerial biomass afforded apigenin-7-O-beta-d-glycoside, using macroporous resin, Sephadex (TM) LH-20 gel, polyamide resin as well as preparative high-performance liquid chromatography (P-HPLC) columns. Chemical structure was elucidated using HPLC/ESI-MS (electrospray ionization-mass spectrometry), Fourier transform infrared (FTIR), and D-1- and D-2-nuclear magnetic resonance (NMR). Apigenin-7-O-beta-d-glycoside could be the post-harvesting product from E. splendens biomass.
引用
收藏
页码：447 / 454
页数：8
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