Synthesis, characterization, and X-ray crystal structures of oxovanadium(V) complexes with hydrazone and 8-hydroxyquinoline ligands

被引：0
|
作者：
Qian, S. S. [1 ]
Ye, Y. T. [2 ]
Ren, J. Q. [2 ]
You, Z. [2 ]
Zhu, H. L. [1 ]
机构：
[1] Shandong Univ Technol, Sch Life Sci, Zibo 25504, Peoples R China
[2] Liaoning Normal Univ, Dept Chem & Chem Engn, Dalian 116029, Peoples R China
来源：
RUSSIAN JOURNAL OF COORDINATION CHEMISTRY | 2014年 / 40卷 / 12期
关键词：
HELICOBACTER-PYLORI UREASE; VANADIUM COMPLEXES; SOLUTION CHEMISTRY; SCHIFF-BASE; INHIBITION; HYDROXAMATE;
D O I：
10.1134/S1070328414120112
中图分类号：
O61 [无机化学];
学科分类号：
070301 ; 081704 ;
摘要：
Three new oxovanadium(V) complexes with the general formula [VO(L) (n) (HQ)] (n = 1-3) were prepared by the reaction of [VO(Acac)(2)] (Acac = acetylacetonate) and 8-hydroxyquinoline with similar benzohydrazide ligands in methanol. Crystal and molecular structures of the complexes were determined by elemental analysis, infrared and UV-Vis spectra and single crystal X-ray diffraction (CIF file CCDC nos. 1004087 (I), 1004088 (II), and 1004089 (III)). The V atoms are in octahedral coordination. Thermal stability of the complexes were studied.
引用
收藏
页码：948 / 953
页数：6
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