Enlargement test of synthesis of MCM-22 zeolite by means of XRD

被引：0
|
作者：
Shi Jian-gong [1 ]
Lu Guan-zhong
Cao Gang
Yu Xiao-dong
机构：
[1] E China Univ Sci & Technol, Res Inst Ind Catalysis, Shanghai 200237, Peoples R China
[2] SINOPEC, Beijing Yanshan Petrochem Corp, Div Chem, Beijing 102500, Peoples R China
[3] SINOPEC, Beijing Yanshan Petrochem Corp, Xingye Tech Dev Corp, Beijing 102500, Peoples R China
来源：
SPECTROSCOPY AND SPECTRAL ANALYSIS | 2007年 / 27卷 / 05期
关键词：
MCM-22; zeolite; hydrothermal synthesis; enlargement test; lattice parameter; XRD;
D O I：
暂无
中图分类号：
O433 [光谱学];
学科分类号：
0703 ; 070302 ;
摘要：
On the basis of MCM-22 zeolite synthesis at the static condition in 100 mL lined PTFE autoclave, 250 and 1 000 mL stainless steel autoclave respectively, the synthesis of MCM-22 zeolite was studied at the rotating condition in 2, 5 and 200 L autoclave respectively. The samples as-synthesized and calcined were characterized by means of XRD and so on. The results show that all the synthesized samples are the pure MCM-22 zeolites, and their crystallinities were high, and MCM-22 zeolite can be synthesized successfully at the rotating condition in 200 L stainless steel autoclave.
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页码：1032 / 1035
页数：4
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