Synthesis of 4′-acetyl(benzo-15-crown-5)-oxime and its complexes with copper(II), nickel(II), cobalt(II) and uranyl(VI)

被引：0

作者：

Avciata, U ^{[1
]}

Demirhan, N ^{[1
]}

Bozdogan, AE ^{[1
]}

机构：

[1] Yildiz Tech Univ, Dept Chem, TR-80270 Istanbul, Turkey

来源：

SYNTHESIS AND REACTIVITY IN INORGANIC AND METAL-ORGANIC CHEMISTRY | 1998年 / 28卷 / 03期

关键词：

D O I：

暂无

中图分类号：

O61 [无机化学];

学科分类号：

070301 ; 081704 ;

摘要：

A new macrocyclic ligand (HL) has been synthesized by the reaction of 4'-acetyl(benzo-15-crown-5) with hydroxylamine hydrochloride. The copper(II), nickel(II), cobalt(II) and uranyl(VI) complexes of the 4'-acetyl(benzo-15-crown-5)oxime (16-acetylhydroxyimino-2,3,5,6,8,9,11,12-octahydrobenzo(1,4,7,10,13)pentaoxacyclopentadecine) have been prepared, characterized and studied potentiometrically at 25 degrees C, I = 1.0 M KNO3. Protonation constants of the ligand and overall formation constants have been calculated from potentiometric data using the program TITFIT.

引用

页码：393 / 403

页数：11

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