Solvothermal synthesis, structure and photoluminescent properties of europium complex based on fluorene derivatives

被引：6
|
作者：
Li, Xing [1 ]
Zha, Mei-Qin [1 ]
Liu, Yan [2 ]
Han, Lei [1 ]
Lv, Hong-Fei [3 ]
机构：
[1] Ningbo Univ, Fac Mat Sci & Chem Engn, State Key Lab Base Novel Funct Mat & Preparat Sci, Ningbo 315211, Zhejiang, Peoples R China
[2] Shanghai Jiao Tong Univ, Sch Chem & Chem Technol, Shanghai 200240, Peoples R China
[3] Heilongjiang Acad Sci, Inst Petrochem, Harbin 150040, Heilongjiang, Peoples R China
来源：
INORGANIC CHEMISTRY COMMUNICATIONS | 2010年 / 13卷 / 09期
基金：
中国国家自然科学基金;
关键词：
Fluorene derivatives; Coordination polymer; Topological structure; Photoluminescence; LANTHANIDE COORDINATION POLYMERS; LIGHT-EMITTING-DIODES; HYDROTHERMAL SYNTHESIS; ACID; LUMINESCENCE; LIGANDS; DEVICES;
D O I：
10.1016/j.inoche.2010.06.028
中图分类号：
O61 [无机化学];
学科分类号：
070301 ; 081704 ;
摘要：
A novel coordination polymer, {[Eu(2)(L)(3)(CH(3)OH)(H(2)O)]center dot(CH(3)OH)(H(2)O)}(n) (1), has been synthesized by solvothermal reaction of Eu( NO(3))(3)center dot 6H(2)O and 9,9-diethylfluorene-2,7-dicarboxylic acid in a mixture solution of CH(3)OH and H(2)O. Single crystal X-ray structural analysis reveals that complex 1 crystallizes in an orthorhombic, space group P2(1)2(1)2(1), holding the unusual (2,3,8)-connected 3D topological network. Thermogravimetric analysis shows remarkable thermal stability of the structural framework of compound 1, the photoluminescence properties are also discussed. (C) 2010 Elsevier B.V. All rights reserved.
引用
收藏
页码：1093 / 1095
页数：3
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