Microwave-assisted rapid synthesis of thiosemicarbazide derivatives

被引：0

作者：

Zamani, K ^{[1
]}

Faghihi, K ^{[1
]}

Bagheri, S ^{[1
]}

Kalhor, M ^{[1
]}

机构：

[1] Arak Univ, Dept Chem, Arak 3815688349, Iran

来源：

INDIAN JOURNAL OF CHEMISTRY SECTION B-ORGANIC CHEMISTRY INCLUDING MEDICINAL CHEMISTRY | 2004年 / 43卷 / 12期

关键词：

D O I：

暂无

中图分类号：

O62 [有机化学];

学科分类号：

070303 ; 081704 ;

摘要：

Rapid and highly efficient synthesis of thiosemicarbazides by the coupling of,isothiocyanate and carboxylic acid hydrazides in small amount of a polar solvent is achieved under microwave irradiation by using a domestic microwave oven. The reaction proceeds rapidly and is completed within 2-4 min giving a series of thiosemicarbazides derivatives 4, 5 in high,yields. All of the compounds have been characterized by FF-IR, H-1- NMR, and mass spectroscopy.

引用

页码：2716 / 2718

页数：3

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