Purification and characterization of single-walled carbon nanotubes produced by arc-discharge

被引：4
|
作者：
Wang, XQ
Wang, M [1 ]
Li, ZH
Zhu, HB
Wang, FF
机构：
[1] Zhejiang Univ, Dept Phys, Hangzhou 310027, Peoples R China
[2] Zhejiang Univ, Micro Syst Ctr Res & Dev, Hangzhou 310027, Peoples R China
[3] Zhejiang Univ, Dept Mech, Hangzhou 310027, Peoples R China
来源：
ACTA PHYSICO-CHIMICA SINICA | 2003年 / 19卷 / 05期
关键词：
single-walled carbon nanotube (SWCNT); microporous membrane; arc-discharge; thermogravimetric analysis (TGA); Raman spectrum;
D O I：
10.3866/PKU.WHXB20030510
中图分类号：
O64 [物理化学（理论化学）、化学物理学];
学科分类号：
070304 ; 081704 ;
摘要：
A purification procedure using microporous membrane and oxidation in air for single-walled carbon nanotubes(SWCNTs) prepared by arc-discharge was discussed which eliminated coexisting metal nanoparticles, carbon nanoparticles and other impurities. The characterization of SWCNTs was carried out at different steps of the purification by TGA, HRTEM and Raman spectra. Experiments show that the method we used is effective to purify the SWCNTs produced by arc-discharge, SWCNTs with the purity of more than 90% could be obtained.
引用
收藏
页码：428 / 431
页数：4
相关论文
共 18 条
  • [1] Purification and characterization of single-wall carbon nanotubes
    Chiang, IW
    Brinson, BE
    Smalley, RE
    Margrave, JL
    Hauge, RH
    [J]. JOURNAL OF PHYSICAL CHEMISTRY B, 2001, 105 (06): : 1157 - 1161
  • [2] Nanotube nanodevice
    Collins, PG
    Zettl, A
    Bando, H
    Thess, A
    Smalley, RE
    [J]. SCIENCE, 1997, 278 (5335) : 100 - 103
  • [3] Dillon AC, 1999, ADV MATER, V11, P1354, DOI 10.1002/(SICI)1521-4095(199911)11:16<1354::AID-ADMA1354>3.0.CO
  • [4] 2-N
  • [5] SINGLE-SHELL CARBON NANOTUBES OF 1-NM DIAMETER
    IIJIMA, S
    ICHIHASHI, T
    [J]. NATURE, 1993, 363 (6430) : 603 - 605
  • [6] A new purification method of single-wall carbon nanotubes using H2S and O2 mixture gas
    Jeong, T
    Kim, WY
    Hahn, YB
    [J]. CHEMICAL PHYSICS LETTERS, 2001, 344 (1-2) : 18 - 22
  • [7] Large-scale production of single-walled carbon nanotubes by the electric-arc technique
    Journet, C
    Maser, WK
    Bernier, P
    Loiseau, A
    delaChapelle, ML
    Lefrant, S
    Deniard, P
    Lee, R
    Fischer, JE
    [J]. NATURE, 1997, 388 (6644) : 756 - 758
  • [8] Nanotube molecular wires as chemical sensors
    Kong, J
    Franklin, NR
    Zhou, CW
    Chapline, MG
    Peng, S
    Cho, KJ
    Dai, HJ
    [J]. SCIENCE, 2000, 287 (5453) : 622 - 625
  • [9] Synthesis of large quantity single-walled carbon nanotubes by arc discharge
    Li, ZH
    Wang, M
    Wang, XQ
    Zhu, HB
    Lu, HM
    Ando, Y
    [J]. CHINESE PHYSICS LETTERS, 2002, 19 (01) : 91 - 93
  • [10] AC impedance analysis of supercapacitors utilizing carbon nanotube electrodes
    Liang, K
    Chen, A
    Feng, ZS
    Ye, ZX
    [J]. ACTA PHYSICO-CHIMICA SINICA, 2002, 18 (04) : 381 - 384
12