Synthesis and characterization of tin sulfates and oxide sulfate

被引：14
|
作者：
Ahmed, MAK [1 ]
Fjellvag, H [1 ]
Kjekshus, A [1 ]
机构：
[1] Univ Oslo, Dept Chem, N-0315 Oslo, Norway
来源：
ACTA CHEMICA SCANDINAVICA | 1998年 / 52卷 / 03期
关键词：
D O I：
10.3891/acta.chem.scand.52-0305
中图分类号：
Q5 [生物化学]; Q7 [分子生物学];
学科分类号：
071010 ; 081704 ;
摘要：
The reactions between metastannic acid, powdered or granulated tin and 50-95 wt% H2SO4 are studied at and above room temperature, and with or without passing oxygen through the reaction mixtures. At least six different solid products, in addition to minor amounts of sulfur as a by-product, are obtained depending on H2SO4 concentration, reaction temperature, reaction atmosphere and tin form. TG and DTA curves are interpreted, unit-cell dimensions are derived from PXD data, and formulae based on chemical and TG analyses are given for the synthesized products.
引用
收藏
页码：305 / 311
页数：7
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