Synthesis, characterization and structural elucidation of monoorgano di(chloro) tin(IV) complexes of heterocyclic dithiocarbamates

被引:0
|
作者
Sharma, J [1 ]
Singh, YP [1 ]
Rai, AK [1 ]
机构
[1] Univ Rajasthan, Dept Chem, Jaipur 302004, Rajasthan, India
来源
MAIN GROUP METAL CHEMISTRY | 2000年 / 23卷 / 05期
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中图分类号
O61 [无机化学];
学科分类号
070301 ; 081704 ;
摘要
Some new monoorganodichlorotin(IV) complexes of heterocyclic dithiocarbamates RCl2Sn[S2CNCH2CH2(X)CH2CH2] (where R = n-C4H9 and C6H5; X CH2, CH-CH3, N-CH3 and O) have been synthesized by the reactions of monoorganotin(IV) trichloride with the sodium saft of heterocyclic dithiocarbamates in 1 : 1 molar ratio in refluxing benzene solution. These complexes have been characterized on the basis of elemental analyses, molecular weight measurements, IR and NMR (H-1, C-13 and Sn-119) spectral studies.
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页码:317 / 320
页数:4
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