CHEMICAL PROFILE OF BEANS CULTIVARS (Phaseolus vulgaris) BY 1H NMR - HIGH RESOLUTION MAGIC ANGLE SPINNING (HR-MAS).

被引:11
|
作者
Liao, Luciano Morais [1 ]
Choze, Rafael [1 ]
Araujo Cavalcante, Pedro Paulo [1 ]
Santos, Suzana da Costa [1 ]
Ferri, Pedro Henrique [1 ]
Ferreira, Antonio Gilberto [2 ]
机构
[1] Univ Fed Goias, Inst Quim, BR-74001970 Goiania, Go, Brazil
[2] Univ Fed Sao Carlos, Dept Quim, BR-13565905 Sao Carlos, SP, Brazil
来源
QUIMICA NOVA | 2010年 / 33卷 / 03期
关键词
H-1 HR-MAS NMR technique; Phaseolus vulgaris; multivariate statistical analysis; MAGNETIC-RESONANCE-SPECTROSCOPY; NMR; LIGANDS; PROTEIN; FLOURS;
D O I
10.1590/S0100-40422010000300028
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
CHEMICAL PROFILE OF BEANS CULTIVARS (Phaseolus vulgaris) BY H-1 NMR - HIGH RESOLUTION MAGIC ANGLE SPINNING (HR-MAS). The application of one-dimensional proton high-resolution magic angle spinning (H-1 HR-MAS) NMR combined with a typical advantages of solid and liquid-state NMR techniques was used as input variables for the multivariate statistical analysis. In this paper, different cultivars of beans (Phaseolus vulgaris) developed and in development by Embrapa - Arroz e Feijdo were analyzed by H-1 HR-MAS, which have been demonstrated to be a valuable tool in its differentiation according chemical composition and avoid the manipulation of the samples as used in other techniques.
引用
收藏
页码:634 / 638
页数:5
相关论文
共 50 条
  • [1] Application of high-resolution-magic-angle-spinning (HR-MAS) NMR spectroscopy to cosmetic emulsions
    Tseng, LH
    Emeis, D
    Raitza, M
    Händel, H
    Albert, K
    [J]. ZEITSCHRIFT FUR NATURFORSCHUNG SECTION B-A JOURNAL OF CHEMICAL SCIENCES, 2000, 55 (07): : 651 - 656
  • [2] Metabolic Profiling of Cells in Response to Drug Treatment using 1H High-resolution Magic Angle Spinning (HR-MAS) NMR Spectroscopy
    Vermathen, Martina
    Diserens, Gaelle
    Vermathen, Peter
    Furrer, Julien
    [J]. CHIMIA, 2017, 71 (03) : 124 - 129
  • [3] 1H high-resolution magic-angle spinning (HR-MAS) NMR analysis of ligand density on resins using a resin internal standard
    Lucas, LH
    Cerny, MA
    Koen, YM
    Hanzlik, RP
    Larive, CK
    [J]. ANALYTICAL AND BIOANALYTICAL CHEMISTRY, 2004, 380 (04) : 627 - 631
  • [4] 1H high-resolution magic-angle spinning (HR-MAS) NMR analysis of ligand density on resins using a resin internal standard
    Laura H. Lucas
    Matthew A. Cerny
    Yakov M. Koen
    Robert P. Hanzlik
    Cynthia K. Larive
    [J]. Analytical and Bioanalytical Chemistry, 2004, 380 : 627 - 631
  • [5] Exploring High-resolution Magic Angle Spinning (HR-MAS) NMR Spectroscopy for Metabonomic Analysis of Apples
    Vermathen, Martina
    Marzorati, Mattia
    Vermathen, Peter
    [J]. CHIMIA, 2012, 66 (10) : 747 - 751
  • [6] Characterization of intervertebral disc degeneration by high-resolution magic angle spinning (HR-MAS) Spectroscopy
    Keshari, KR
    Zektzer, AS
    Swanson, MG
    Majumdar, S
    Lotz, JC
    Kurhanewicz, J
    [J]. MAGNETIC RESONANCE IN MEDICINE, 2005, 53 (03) : 519 - 527
  • [7] High-Resolution Magic Angle Spinning (HR-MAS) NMR-Based Fingerprints Determination in the Medicinal PlantBerberis laurina
    Ali, Sher
    Badshah, Gul
    Da Ros Montes D'Oca, Caroline
    Ramos Campos, Francinete
    Nagata, Noemi
    Khan, Ajmir
    de Fatima Costa Santos, Maria
    Barison, Andersson
    [J]. MOLECULES, 2020, 25 (16):
  • [8] High resolution-magic angle spinning (HR-MAS) NMR-based metabolomic fingerprinting of early and recurrent hepatocellular carcinoma
    Antonio Solinas
    Matilde Chessa
    Nicola Culeddu
    Maria Cristina Porcu
    Giuseppe Virgilio
    Francesco Arcadu
    Angelo Deplano
    Sergio Cossu
    Domenico Scanu
    Vincenzo Migaleddu
    [J]. Metabolomics, 2014, 10 : 616 - 626
  • [9] High resolution-magic angle spinning (HR-MAS) NMR-based metabolomic fingerprinting of early and recurrent hepatocellular carcinoma
    Solinas, Antonio
    Chessa, Matilde
    Culeddu, Nicola
    Porcu, Maria Cristina
    Virgilio, Giuseppe
    Arcadu, Francesco
    Deplano, Angelo
    Cossu, Sergio
    Scanu, Domenico
    Migaleddu, Vincenzo
    [J]. METABOLOMICS, 2014, 10 (04) : 616 - 626
  • [10] Metabolic profiling of apples from different production systems before and after controlled atmosphere (CA) storage studied by 1H high resolution-magic angle spinning (HR-MAS) NMR
    Vermathen, Martina
    Marzorati, Mattia
    Diserens, Gaelle
    Baumgartner, Daniel
    Good, Claudia
    Gasser, Franz
    Vermathen, Peter
    [J]. FOOD CHEMISTRY, 2017, 233 : 391 - 400