RETRACTED: Synthesis of ZrB2-SiC ceramic composites from a single-source precursor (Retracted Article)

被引：9

作者：

Arish, Dasan ^{[1
]}

Shiju, Chellan ^{[2
]}

Joseyphus, Raphael Selwin ^{[3
]}

Pushparajan, Joseph ^{[4
]}

机构：

[1] Univ Limoges, SPCTS CNRS, UMR 7315, CEC, 12 Rue Atlantis, F-87068 Limoges, France

[2] HLL Lifecare Ltd, CRDC, Synthet Prod Div, Thiruvananthapuram, Kerala, India

[3] Mar Ivanios Coll Autonomous, Dept Chem, PG & Res, Thiruvananthapuram 695015, Kerala, India

[4] Travancore Titanium Prod Ltd, Thiruvananthapuram 695021, Kerala, India

来源：

MATERIALS CHEMISTRY AND PHYSICS | 2017年 / 194卷

关键词：

Preceramic polymer; ZrB2-SiC; IR; Raman; SEM; LOW-TEMPERATURE SYNTHESIS; DIBORIDE-SILICON CARBIDE; POLYMER-DERIVED CERAMICS; SOL-GEL SYNTHESIS; ZIRCONIUM DIBORIDE; MECHANICAL-PROPERTIES; RAMAN-SPECTRUM; CARBON; OXIDATION; ZR;

D O I：

10.1016/j.matchemphys.2017.03.055

中图分类号：

T [工业技术];

学科分类号：

08 ;

摘要：

Preceramic polymer zirconoborosiloxane was synthesized from the reaction with boric acid, diphenyldiethoxysilane and zirconium (IV) propoxide via solventless process. The thermogravimetric analysis of the polymer showed that ceramic yield as decomposition product at 900 degrees C was 71%. The pyrolysis of zirconoborosiloxane in an argon gas environment was investigated as standard pyrolytic process up to 1650 degrees C. Microstructure evolution of ceramic phases was made by means of Fourier transform infrared, Raman spectroscopy, X-ray diffraction and scanning electron microscope analysis. The results clearly demonstrated the pyrolysis products at 1650 degrees C consist of totally non-oxide ceramic phases beta-SIC, ZrB2 and free carbon. (C) 2017 Elsevier B.V. All rights reserved.

引用

页码：308 / 312

页数：5

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[1] RETRACTION: Synthesis of ZrB2-SiC ceramic composites from a single-source precursor (Retraction of Vol 194, Pg 308, 2017)
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