Covalently anchored sulfonic acid onto silica as an efficient and recoverable interphase catalyst for the synthesis of 3,4-dihydropyrimidinones/thiones

被引：93

作者：

Gupta, Raman ^{[1
]}

Paul, Satya ^{[1
]}

Gupta, Rajive ^{[1
]}

机构：

[1] Univ Jammu, Dept Chem, Jammu 180006, India

来源：

JOURNAL OF MOLECULAR CATALYSIS A-CHEMICAL | 2007年 / 266卷 / 1-2期

关键词：

sulfonic acid functionalized silica; Biginelli reaction; re-usable heterogeneous catalyst; green procedure; solid-liquid phase catalysis;

D O I：

10.1016/j.molcata.2006.10.039

中图分类号：

O64 [物理化学（理论化学）、化学物理学];

学科分类号：

070304 ; 081704 ;

摘要：

A novel covalently anchored sulfonic acid onto the surface of silica was prepared and investigated for the Biginelli reaction. The catalyst is highly stable, completely heterogeneous and recyclable for several times. The work-up procedure is very simple and Biginelli compounds were obtained in good to excellent yields. (c) 2006 Elsevier B.V. All rights reserved.

引用

页码：50 / 54

页数：5

共 50 条

[1] Silica-based sulfonic acid (SiO2-Pr-SO3H): an efficient catalyst in the green one-pot synthesis of 3,4-dihydropyrimidinones/thiones
Ziarani, G. Mohammadi
Badiei, A.
Lashgari, N.
Pourjafar, T.
Farahani, Z.
BULGARIAN CHEMICAL COMMUNICATIONS, 2014, 46 (04): : 719 - 723
[2] Synthesis and characterization of nano acid catalyst derived from rice husk silica and its application for the synthesis of 3,4-dihydropyrimidinones/thiones compounds
Davarpanah, Jamal
Sayahi, Mohammad Hosein
Ghahremani, Mahboubeh
Karkhoei, Sahar
JOURNAL OF MOLECULAR STRUCTURE, 2019, 1181 : 546 - 555
[3] A bipyridyl palladium complex covalently anchored onto silica as an effective and recoverable interphase catalyst for the aerobic oxidation of alcohols
Karimi, B
Zamani, A
Clark, JH
ORGANOMETALLICS, 2005, 24 (19) : 4695 - 4698
[4] Silica-gel Catalyzed Facile Synthesis of 3,4-Dihydropyrimidinones
Agarwal, Sameer
Aware, Umesh
Patil, Amit
Rohera, Vinita
Ghate, Manjunath
Jain, Mukul
Patel, Pankaj
BULLETIN OF THE KOREAN CHEMICAL SOCIETY, 2012, 33 (02): : 377 - 378
[5] Synthesis, Antileishmanial Activity and Molecular Docking Study of New 3,4-Dihydropyrimidinones/Thiones
Mohammadi-Ghalehbin, Behnam
Sepehri, Saghi
Nejatkhah, Negin
Safari, Sahand
Hosseinali, Zahra
Sabour, Sahar
Razzaghi-Asl, Nima
PHARMACEUTICAL CHEMISTRY JOURNAL, 2022, 55 (10) : 1050 - 1056
[6] Synthesis, Antileishmanial Activity and Molecular Docking Study of New 3,4-Dihydropyrimidinones/Thiones
Behnam Mohammadi-Ghalehbin
Saghi Sepehri
Negin Nejatkhah
Sahand Safari
Zahra Hosseinali
Sahar Sabour
Nima Razzaghi-Asl
Pharmaceutical Chemistry Journal, 2022, 55 : 1050 - 1056
[7] Green synthesis of 3,4-dihydropyrimidinones using nano Fe3O4@meglumine sulfonic acid as a new efficient solid acid catalyst under microwave irradiation
Moradi, Leila
Tadayon, Maryam
JOURNAL OF SAUDI CHEMICAL SOCIETY, 2018, 22 (01) : 66 - 75
[8] Solid silica-based sulfonic acid as an efficient and recoverable interphase catalyst for selective tetrahydropyranylation of alcohols and phenols
Karimi, B
Khalkhali, M
JOURNAL OF MOLECULAR CATALYSIS A-CHEMICAL, 2005, 232 (1-2) : 113 - 117
[9] Zirconia Sulfuric Acid: An Efficient Heterogeneous Catalyst for the One-Pot Synthesis of 3,4-Dihydropyrimidinones Under Solvent-Free Conditions
Maliheh M. Hosseini
Eskandar Kolvari
Nadiya Koukabi
Maryam Ziyaei
Mohammad Ali Zolfigol
Catalysis Letters, 2016, 146 : 1040 - 1049
[10] Zirconia Sulfuric Acid: An Efficient Heterogeneous Catalyst for the One-Pot Synthesis of 3,4-Dihydropyrimidinones Under Solvent-Free Conditions
Hosseini, Maliheh M.
Kolvari, Eskandar
Koukabi, Nadiya
Ziyaei, Maryam
Zolfigol, Mohammad Ali
CATALYSIS LETTERS, 2016, 146 (06) : 1040 - 1049

← 1 2 3 4 5 →