Comparison of DI-SPME-GC-MS and SPE-GC-MS with Derivatization for Analysis of Steroid Hormones in River Water

被引：0
|
作者：
Miclean, Mirela [1 ]
Senila, Lacrimioara [1 ]
Roman, Cecilia [1 ]
Gog, Adriana [1 ]
Levei, Erika Andrea [1 ]
Groza, Ioan [2 ]
机构：
[1] Res Inst Analyt Instrumentat, INCDO INOE 2000, Cluj Napoca 400293, Romania
[2] Univ Agr Sci & Vet Med, Cluj Napoca 400372, Romania
来源：
REVISTA DE CHIMIE | 2010年 / 61卷 / 06期
关键词：
steroid hormones; SPME; SPE; MSTFA; GC-MS; Somes River; ENDOCRINE-DISRUPTING CHEMICALS; PHASE MICROEXTRACTION; DEGRADATION;
D O I：
暂无
中图分类号：
O6 [化学];
学科分类号：
0703 ;
摘要：
In this study two extraction methods were performed for analysis of estrone and beta-estradiol in wastewater effluent and Somes River water: solid-phase microextraction (SPME) and solid phase extraction (SPE), both followed by gas chromatography - mass spectrometry (GC-MS). The target compounds were detected in water samples collected downstream of municipal sewage treatment plant of Cluj-Napoca, Romania. The results obtained by SPME and SPE methods for analyzed samples were of the same order of magnitude.
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页码：615 / 618
页数：4
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